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Chemical Structure| 183070-44-2 Chemical Structure| 183070-44-2
Chemical Structure| 183070-44-2

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CAS No.: 183070-44-2

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Product Details of [ 183070-44-2 ]

CAS No. :183070-44-2
Formula : C29H29NO6
M.W : 487.54
SMILES Code : O=C(O)[C@@H](NC(OCC1C2=C(C3=C1C=CC=C3)C=CC=C2)=O)CC4=CC=C(C(OC(C)(C)C)=O)C=C4
MDL No. :MFCD01317016
InChI Key :GQIVAZYTLZQGHT-VWLOTQADSA-N
Pubchem ID :21345475

Safety of [ 183070-44-2 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338

Application In Synthesis of [ 183070-44-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 183070-44-2 ]

[ 183070-44-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 23357-46-2 ]
  • [ 183070-44-2 ]
  • tert-butyl 4-((S)-2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-oxo-3-(((R)-1,2,3,4-tetrahydronaphthalen-1-yl)amino)propyl)benzoate [ No CAS ]
YieldReaction ConditionsOperation in experiment
To a 00 C. solution of (S)-2-((((9H-fluoren-9-yl) methoxy)carbonyl)amino)-3-(4-(tert-butoxycarbonyl)phe- nyl)propanoic acid (Chem-Impex, 150 mg, 0.308 mmol) in DMF (2051 pi) was added EDC (70.8 mg, 0.369 mmol) followed by 3H-[1 ,2,3] -triazolo[4,5-b]pyridin-3-ol (50.3 mg, 0.369 mmol). Afier 10 mi (R)-1,2,3,4-tetrahydronaph- thalen- 1-amine (45.2 pi, 0.308 mmol) and N-methylmorpholine (101 pi, 0.923 mmol) were added and the resulting reaction mixture was allowed to warm to it slowly overnight. The reaction mixture was then diluted with EtOAc and washed with iN HC1 (2x) and 10% EiC1 (lx). The organic layer was then dried over MgSO4, filtered, and concentrated in vacuo to give crude tert-butyl 4-((S)-2- ((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-oxo-3- (((R)-1 ,2,3,4-tetrahydronaphthalen-1 -yl)amino)propyl)benzoate (177 mg, 0.287 mmol, 93% yield) as a clear oil, which was used without further purification. MS(ESI) mlz 617.5 (M+H).
 

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[ 183070-44-2 ]

Chemical Structure| 2973755-09-6

A1398662 [2973755-09-6]

(R)-2-((((9H-Fluoren-9-yl)methoxy)carbonyl)amino)-3-(4-(tert-butoxycarbonyl)phenyl)propanoic acid

Reason: Optical isomers