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CAS No. : | 17773-10-3 | MDL No. : | MFCD00011900 |
Formula : | C5H14INO | Boiling Point : | No data available |
Linear Structure Formula : | - | InChI Key : | FNPBHXSBDADRBT-UHFFFAOYSA-M |
M.W : | 231.08 | Pubchem ID : | 87300 |
Synonyms : |
|
Chemical Name : | Choline Iodide |
Signal Word: | Warning | Class: | |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | |
Hazard Statements: | H315-H319-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With pillar[5]arene; acetylcholinesterase; at 37℃; for 1.5h; | The hydrolysis percentageof G2 in the absence and presence ofWP5 by culturing with AChE at 37 °Cfor different times was monitored by 1H NMR experiments. Theconcentrations of G2, WP5 and AChE were 30 mM, 30 mM and 1 U/ml, respectively. The accuratehydrolysis percentage could be determined by calculating the peak area ratio ofthe protons on choline iodide (G1)and <strong>[2260-50-6]acetylcholine iodide</strong> (G2) |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
93% | at 65℃; for 2.0h; | Add 3 mol of 3,5-dihydroxy-4-acetyltoluene and 5 mol of iodocholine to the reaction vessel to control the stirring speed.130rpm, raise the temperature to 65 ° C, maintain the temperature and continue to stir until completely dissolved, let stand for 120min, reduce the solution temperatureThe crystal was precipitated to 15 ° C, filtered, and the crystal was washed with a cyclohexane solution having a mass fraction of 85percent, and the mass fraction was 90percent.The toluene solution was washed, and the anhydrous potassium carbonate dehydrating agent was dehydrated to obtain 761.67 g of the finished iodoacetylcholine, and the yield was 93percent |