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Chemical Structure| 17252-51-6 Chemical Structure| 17252-51-6
Chemical Structure| 17252-51-6

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CAS No.: 17252-51-6

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Product Details of [ 17252-51-6 ]

CAS No. :17252-51-6
Formula : C13H14N2
M.W : 198.26
SMILES Code : C1(CCCC2=CC=NC=C2)=CC=NC=C1
MDL No. :MFCD00038046
InChI Key :OGNCVVRIKNGJHQ-UHFFFAOYSA-N
Pubchem ID :87019

Safety of [ 17252-51-6 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302+H312+H332-H315-H319-H335
Precautionary Statements:P261-P280-P305+P351+P338

Application In Synthesis of [ 17252-51-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 17252-51-6 ]

[ 17252-51-6 ] Synthesis Path-Downstream   1~18

  • 1
  • iron(II) nitrate [ No CAS ]
  • [ 17252-51-6 ]
  • [ 7732-18-5 ]
  • [ 68-04-2 ]
  • [Fe4(citrate)4(H2O)4][1,3-bis(4-pyridyl)propane(+2H)]2*H2O [ No CAS ]
  • 2
  • [ 17252-51-6 ]
  • [ 499-49-0 ]
  • [ 6147-53-1 ]
  • [Co2(5-methylisophthalate)2(1,3-bis(4-bipyridyl)propane)2(H2O)]n [ No CAS ]
  • 3
  • zinc(II) nitrate hexahydrate [ No CAS ]
  • [ 17252-51-6 ]
  • [ 610-09-3 ]
  • [Zn2(μ-e,a-cis-1,2-cyclohexanedicarboxylate)2(μ-1,3-bis(4-pyridyl)propane)2Zn2(μ-cis-1,2-C6H10(CO2)2)2(H2O)2]*MeCN*2H2O [ No CAS ]
  • 4
  • [ 17252-51-6 ]
  • cadmium(II) nitrate tetrhydrate [ No CAS ]
  • [ 23351-91-9 ]
  • [ 7732-18-5 ]
  • [ 1260529-86-9 ]
  • 5
  • [ 17252-51-6 ]
  • [ 23351-91-9 ]
  • [ 7732-18-5 ]
  • [ 6156-78-1 ]
  • poly[tetrakis(5-bromoisophthalato)bis(4-(3-(4-pyridyl)propyl)pyridinium)(aqua)trimanganese(II) monohydrate] [ No CAS ]
  • 6
  • [ 17252-51-6 ]
  • [ 23351-91-9 ]
  • [ 6018-89-9 ]
  • [ 1379609-53-6 ]
  • 7
  • [ 17252-51-6 ]
  • [ 23351-91-9 ]
  • [ 6147-53-1 ]
  • [ 1379609-52-5 ]
  • 8
  • cobalt(II) nitrate hexahydrate [ No CAS ]
  • [ 17252-51-6 ]
  • [ 569-51-7 ]
  • [ 7732-18-5 ]
  • [tetracobalt(II)(μ3-OH)2(1,2,3-benzenetricarboxylate)2(1,3-bis(4-pyridyl)propane)2(H2O)2]*1,3-bis(4-pyridyl)propane [ No CAS ]
  • 9
  • nickel(II) nitrate hexahydrate [ No CAS ]
  • [ 17252-51-6 ]
  • [ 7732-18-5 ]
  • [ 68-12-2 ]
  • [ 130-85-8 ]
  • [Ni(PA)(bpp)(H2O)2]DMF}n [ No CAS ]
YieldReaction ConditionsOperation in experiment
36% In methanol; at 110℃; for 72h;High pressure; 2.2.4 [Ni(PA)(bpp)(H2O)2]·DMF}n (4) (0007) A mixture of Ni(NO3)2·6H2O (0.291g, 1mmol), H2PA (0.388g, 1mmol), bpp (0.198g, 1mmol) and KOH (0.112g, 2mmol) in DMF?H2O?MeOH (1:2:2) (10mL) was heated for 72h at 110°C in a Teflon-lined stainless steel vessel (23mL). The reaction system was then cooled to room temperature and green block crystals of 4 were collected, washed with water and dried in air (yield 36percent). IR data (KBr, cm?1): 3381m, 3056w, 2931w, 2360m, 1647vs, 1616m, 1569s, 1509m, 1460m, 1401m, 1337s, 1270w, 1231w, 1155w, 1102w, 815m, 755m, 668w, 604w, 526w. Anal. Calc. for C39H39N3NiO9 (752.44): C, 62.20; H, 5.18; N, 5.58. Found: C, 62.27; H, 5.24; N, 5.53percent.
  • 10
  • [ 67-56-1 ]
  • [ 17252-51-6 ]
  • cadmium(II) nitrate tetrhydrate [ No CAS ]
  • [ 130-85-8 ]
  • [Cd(PA)(bpp)(CH3OH)]*CH3OH}n [ No CAS ]
YieldReaction ConditionsOperation in experiment
38% In water; N,N-dimethyl-formamide; at 110℃; for 72h;High pressure; General procedure: 2.2.4 [Ni(PA)(bpp)(H2O)2]·DMF}n (4) (0007) A mixture of Ni(NO3)2·6H2O (0.291g, 1mmol), H2PA (0.388g, 1mmol), bpp (0.198g, 1mmol) and KOH (0.112g, 2mmol) in DMF?H2O?MeOH (1:2:2) (10mL) was heated for 72h at 110°C in a Teflon-lined stainless steel vessel (23mL). The reaction system was then cooled to room temperature and green block crystals of 4 were collected, washed with water and dried in air (yield 36percent).
  • 11
  • [ 14285-68-8 ]
  • [ 17252-51-6 ]
  • [ 1194-22-5 ]
  • [Re2(CO)6(μ-η4-2-methylpyrimidine-4,6-diol)(μ-4,4'-trimethylenedipyridine)] [ No CAS ]
  • 12
  • cobalt(II) nitrate hexahydrate [ No CAS ]
  • [ 17252-51-6 ]
  • [ 499-49-0 ]
  • [ 1378939-40-2 ]
  • 13
  • zinc(II) nitrate hexahydrate [ No CAS ]
  • [ 17252-51-6 ]
  • [ 499-49-0 ]
  • [ 1225267-13-9 ]
  • 14
  • [ 17252-51-6 ]
  • [ 23351-91-9 ]
  • [ 7732-18-5 ]
  • [ 10108-64-2 ]
  • [Cd(5-bromoisophthalate)Cl(H2O)](1,3-bis(4-pyridyl)propane)0.5}n [ No CAS ]
YieldReaction ConditionsOperation in experiment
58% at 140℃; for 72h;High pressure; A mixture of 5-Br-H2ip (24.3mg, 0.1 mmol), bpp (0.1 mmol,18.4 mg), CdCl2 (18.3 mg, 0.1 mmol) and H2O (10 mL) was placed in a Teflon-lined stainless steel vessel, heated to 140 °C for 3 days, and then cooled to room temperature over 24 h. Colorless block crystals of 2 were obtained. Yield: 58percent basedon Cd.
  • 15
  • [ 14285-68-8 ]
  • [ 17252-51-6 ]
  • [ 106-42-3 ]
  • [ 1194-22-5 ]
  • [Re2(CO)6(μ-η4-2-methylpyrimidine-4,6-diol(-2H))(μ-4,4'-trimethylenedipyridine)]*p-xylene [ No CAS ]
  • 16
  • zinc(II) nitrate hexahydrate [ No CAS ]
  • [ 17252-51-6 ]
  • [ 81-16-3 ]
  • [zinc(II)(1,3-bi(4-pyridyl)propane)2(2-aminonaphthalene-1-sulfonate)2]n [ No CAS ]
YieldReaction ConditionsOperation in experiment
32% With sodium hydroxide; In water; at 160℃; for 120h;High pressure; Autoclave; General procedure: For [Zn2(bpp)2(na)4]n(1), a mixture of Hna (68.9 mg,0.4 mmol), bpp (79.2 mg, 0.4 mmol), Zn(NO3)2.6H2O(118.8 mg, 0.4 mmol), NaOH (24.0 mg, 0.6 mmol), and doubly deionized water (12.0 mL) was sealed in a 23.0 mL stainless steel vessel and heated at 160C for 120 hours underautogenous pressure. After the mixture was cooled to roomtemperature at a rate of 5C h-1, colorless block-shaped crystals suitable for single-crystal X-ray diffraction analysis wereisolated directly, washed with ethanol, and dried in air. Yield: 36.0% (based on Hna).
  • 17
  • [ 17252-51-6 ]
  • [ 5743-04-4 ]
  • [ 81-16-3 ]
  • [Cd(1,3-bi(4-pyridyl)propane)2(2-aminonaphthalene-1-sulfonate)2]n [ No CAS ]
YieldReaction ConditionsOperation in experiment
46% With sodium hydroxide; In water; at 140℃; for 72h;High pressure; Autoclave; A mixture of HNas (89.3 mg,0.4 mmol), Bpp (39.6 mg, 0.2 mmol), CdAc2 · 2H2O(106.6 mg, 0.4 mmol), NaOH (24.0 mg, 0.6 mmol),and doubly deionized water (12 mL) were sealed in a23 mL stainless steel vessel. Then the mixture washeated at 140C for 72 h under autogenous pressure.After the mixture was cooled to room temperature atthe rate of 5C h-1, colorless block-shaped crystalssuitable for single-crystal X-ray diffraction analysiswere isolated directly, washed with ethanol, and driedin air. The yield was 46% based on Cd salts.For C46H44N6O6S2Cdanal. calcd., %: C, 57.95; H, 4.65; N, 8.81.Found, %: C, 57.92; H, 4.67; N, 8.83.
  • 18
  • [ 27148-03-4 ]
  • zinc(II) nitrate hexahydrate [ No CAS ]
  • [ 17252-51-6 ]
  • [Zn(1,1-dioxo-1,2-benzisothiazole-3-thiolato)<SUB>2</SUB>(4,4'-trimethylenedipyridine)]<SUB>n</SUB> [ No CAS ]
YieldReaction ConditionsOperation in experiment
82% In ethanol; water; at 20℃; The complex was synthesized by addition of 4,4'-trimethylenedipyridine (6.2 mg, 0.031 mmol) and <strong>[27148-03-4]thiosaccharine</strong> (12.7 mg, 0.0638 mmol), respectively, to a solution of Zn(NO3)26H2O (10.2mg, 0.0342 mmol) in ethanol:water (4 ml), and kept under mechanical stirring at room temperature. The resulting yellow solid was filtered off and washed with cold water. By slow evaporation of the mother solution single crystals appeared. They were washed with water and analysed using X-ray diffraction. Yield: 82%. Molar conductivity (mS M1) = 28.3. Analytical percent composition calculated for C27H22N4O4S4Zn: C = 49.127%; H = 3.359%;N = 8.487%. Found: C = 48.811%; H = 2.981%; N = 8.378%. Soluble in DMSO and DMF. Slightly soluble in water, ethanol, methanol, chloroform. Insoluble in acetone and methane dichloride. UV-Visible [DMSO, kmax nm]: 347.1H NMR (300 MHz, DMSO) d 8.46 (dd, 4H), 7.92 (m, 2H), 7.58-7.72 (m, 6H), 7.28 (dd, 4H), 2.64 (t, 4H), 1.93 (m, 2H). 13C NMR (75 MHz, DMSO) d 191.71 (C1), 151.07 (C10), 149.31 (C8), 137.98(C7), 136.56 (C2), 132.05 (C4), 130.82 (C5), 125.07 (C3), 124.04(C9), 119.01 (C6), 33.80 (C11), 30.12 (C12).
 

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