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[ CAS No. 169624-67-3 ] {[proInfo.proName]}

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Chemical Structure| 169624-67-3
Chemical Structure| 169624-67-3
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Product Details of [ 169624-67-3 ]

CAS No. :169624-67-3 MDL No. :MFCD01318734
Formula : C26H24N2O5 Boiling Point : -
Linear Structure Formula :- InChI Key :WJQWIPAQNBOEBX-QHCPKHFHSA-N
M.W : 444.48 Pubchem ID :11328236
Synonyms :
Chemical Name :Fmoc-Phe-Gly

Safety of [ 169624-67-3 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P305+P351+P338 UN#:N/A
Hazard Statements:H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 169624-67-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 169624-67-3 ]

[ 169624-67-3 ] Synthesis Path-Downstream   1~17

  • 1
  • [ 721-90-4 ]
  • [ 82911-69-1 ]
  • [ 169624-67-3 ]
  • 2
  • [ 29390-67-8 ]
  • [ 169624-67-3 ]
  • 6-<N-(fluoren-9-ylmethoxycarbonyl)-L-phenylalanylglycylamido>-6-deoxycyclomaltoheptaose [ No CAS ]
  • 3
  • [ 169624-67-3 ]
  • [ 351356-27-9 ]
  • methyl N-[(9H-fluoren-9-yl)methoxy]carbonyl}-(S)-phenylalanyl-glycyl-dimethylglycyl-(2S,4R)-4-(benzyloxy)prolinate [ No CAS ]
  • 4
  • [ 169624-67-3 ]
  • [ 445396-16-7 ]
  • methyl N-[(9H-fluoren-9-yl)methoxy]carbonyl}-(S)-phenylalanyl-glycyl-dimethylglycyl-(S)-N-methylvalinate [ No CAS ]
  • 5
  • [ 169624-67-3 ]
  • [ 445396-40-7 ]
  • methyl N-[(9H-fluoren-9-yl)methyoxy]carbonyl}-(S)-phenylalanyl-glycyl-(R/S)-methyl(ethyl)glycyl-(S)-prolinate [ No CAS ]
  • 6
  • [ 68858-20-8 ]
  • [ 35661-39-3 ]
  • [ 108-24-7 ]
  • [ 169624-67-3 ]
  • [ 790692-31-8 ]
  • H-Leu-O-(2-chlorotrityl)polystyrene resin [ No CAS ]
  • Ac-Ala-Phe-Gly-Val-Azy-Leu-O-(2-chlorotrityl)polystyrene resin [ No CAS ]
  • 8
  • [ 68858-20-8 ]
  • [ 35661-39-3 ]
  • [ 108-24-7 ]
  • [ 169624-67-3 ]
  • [ 790692-31-8 ]
  • PhSeH2-chlorotrityl-linked polystyrene-supported leucine [ No CAS ]
  • (S)-2-[(R)-2-((S)-2-{2-[(S)-2-((S)-2-Acetylamino-propionylamino)-3-phenyl-propionylamino]-acetylamino}-3-methyl-butyrylamino)-3-phenylselanyl-propionylamino]-4-methyl-pentanoic acid [ No CAS ]
  • 9
  • [ 35661-60-0 ]
  • [ 169624-67-3 ]
  • [ 1122069-22-0 ]
  • [ 79396-84-2 ]
  • 10
  • [ 1316293-48-7 ]
  • [ 169624-67-3 ]
  • 11
  • [ 35661-40-6 ]
  • [ 169624-67-3 ]
  • 12
  • [ 103321-57-9 ]
  • [ 169624-67-3 ]
  • 13
  • [ 7364-42-3 ]
  • [ 35661-40-6 ]
  • [ 169624-67-3 ]
  • 14
  • [ 17364-16-8 ]
  • [ 169624-67-3 ]
  • 1-palmitoyl-2-(Fmoc-Phe-Gly)-sn-glycero-3-phosphocholine [ No CAS ]
YieldReaction ConditionsOperation in experiment
58% With dmap; dicyclohexyl-carbodiimide; In chloroform; at 25℃; for 48h;Sonication; To a suspension of 1-palmitoyl-2-hydroxy-sn-glycero-3-phos-phocholine 6 (0.5002 g, 1 mmol) in 25 mL of CHCl3 were addedFMOC-phe-gly-OH (0.5393 g, 1.2 mmol), DCC (0.2498 g, 1.2 mmol),DMAP (0.1479 g, 1.2 mmol) and 1 g of glass beads. The reaction wassonicated for 48 h at 25 C, the mixture was thenfiltered to removeDCC-urea and glass beads. The solvent was evaporated to one thirdof the volume and then loaded on a silica gel column forchromatography. A stepwise gradient of CHCl3/MeOH (5:1 and 5:2)was applied to elute DMAP and some impurities, followed byCHCl3/MeOH/H2O (65:25:4). The fractions corresponding to theproduct were combined, evaporated, re-dissolved in benzene andfreeze-dried to give 110 as a white solid (0.5352 g, 0.58 mmol, 58%).IR (Nujol): 3297 br m,1728 vs,1693 s,1654 vs,1536 m,1252 w cm1.1H NMR (CDCl3, 200 MHz) d 0.85 (br t, 3H), 1.25 (br s, 24H),1.50 (m, 2H), 2.20 (t, 2H, J = 6.7 Hz), 2.95 (m, 2H), 3.17 (br s, 9H), 3.67(br s, 2H), 3.95-4.30 (br m, 10H), 4.44 (m, 2H), 5.36 (m, 1H),6.15 (m, 1H), 7.21-7.47 (m, 11H), 7.72 (d, 2H, J = 7.4 Hz), 8.66 (m,1H).13C NMR (CDCl3, 50 MHz) d 14.28, 22.85, 24.92, 29.31, 29.52, 29.71,29.83, 29.87, 32.08, 34.04, 38.94, 41.47, 47.13, 54.34, 55.90, 59.63,62.44, 64.18, 66.28, 67.07, 71.96, 120.08, 125.27, 125.47, 126.94,127.26, 127.86, 128.57, 129.63, 137.05, 141.30, 143.90, 156.17, 169.83,172.39, 173.72. Rf (CHCl3/MeOH/H2O 65:25:4) 0.48. Anal. Cald forC50H72N3O11P2.5H2O C, 62.09; H, 8.02; N, 4.34; found: C, 62.33; H,8.03; N, 4.04. FAB-MS MH+ C50H72N3O11PH Calcd: 922.4977, found:922.4981. [a]D25 C -6.73 (c 0.98, CHCl3/MeOH 4:1).
  • 15
  • [ 169624-67-3 ]
  • C32H37N3O5*C2HF3O2 [ No CAS ]
  • 16
  • [ 169624-67-3 ]
  • C49H62N4O9 [ No CAS ]
  • 17
  • [ 169624-67-3 ]
  • C34H52N4O7 [ No CAS ]
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