Purity | Size | Price | VIP Price | USA Stock *0-1 Day | Global Stock *5-7 Days | Quantity | ||||||
{[ item.p_purity ]} | {[ item.pr_size ]} | Inquiry |
{[ getRatePrice(item.pr_usd, 1,1,item.pr_is_large_size_no_price) ]} {[ getRatePrice(item.pr_usd,item.pr_rate,1,item.pr_is_large_size_no_price) ]} |
{[ getRatePrice(item.pr_usd, 1,1,item.pr_is_large_size_no_price) ]} | Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price) ]} {[ getRatePrice(item.pr_usd,1,item.mem_rate,item.pr_is_large_size_no_price) ]} | {[ item.pr_usastock ]} | in stock Inquiry - | {[ item.pr_chinastock ]} | {[ item.pr_remark ]} in stock Inquiry - | Login | Inquiry |
Please Login or Create an Account to: See VIP prices and availability
CAS No. : | 16114-47-9 | MDL No. : | MFCD02677945 |
Formula : | C5H8BNO3 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | DIIFZCPZIRQDIJ-UHFFFAOYSA-N |
M.W : | 140.93 | Pubchem ID : | 2734346 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
75% | With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In 1,4-dioxane; water; at 140℃; for 0.25h;Inert atmosphere; Microwave irradiation; | 2-Chloroquinoline-4-carboxylic acid (0.15 g, 0.72 mmol), 3,5-dimethylisoxazole-4-boronic acid (0.12 g, 0.87 mmol) and Pd(PPh3)4 (42 mg, 0.04 mmol) were added to a mixture of dioxane (2 mL) and a 1 M aq solution of K2CO3 (2 mL). The reaction mixture was degassed, sealed, and heated in a microwave reactor at 140 °C for 15 min. The reaction mixture was concentrated in vacuo to leave a residue which was purified by HPLC using a gradient of 30-100percent mobile phase A (100percent CH3CN) over 30 min (mobile phase B = 5percent CH3CN + 95percent 0.1 M NH4OAc) to give the intermediate carboxylic acid (148 mg, 75percent). m/z 269.6 (M+H)+. The intermediate carboxylic acid was then coupled to 4 using essentially the same method as for 17 to give the title compound as a solid. 1H NMR (400 MHz, DMSO-d6) delta 8.76 (t, J = 5.5 Hz, 1H), 8.12-8.04 (m, 2H), 7.83 (t, J = 7.3 Hz, 1H), 7.71-7.60 (m, 2H), 6.79 (s, 1H), 3.22 (t, J = 6.0 Hz, 2H), 2.77 (t, J = 6.1 Hz, 2H), 2.69 (s, 3H), 2.50 (s, 3H), 1.81 (d, J = 10.9 Hz, 2H), 1.72 (d, J = 11.6 Hz, 2H), 1.60-1.47 (m, 1H), 1.37 (s, 9H), 1.35-1.26 (m, 1H), 1.05-0.79 (m, 4H); HRMS (ESI) m/z calcd for C28H37N4O4 [M+H]+ 493.2815; found 493.2821. |
[ 832114-00-8 ]
3,5-Dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)isoxazole
Similarity: 0.78
[ 1346808-41-0 ]
5-Methylisoxazole-4-boronic Acid Pinacol Ester
Similarity: 0.69
[ 928664-98-6 ]
4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)isoxazole
Similarity: 0.56
[ 1072952-34-1 ]
(2-Methylpyridin-3-yl)boronic acid hydrochloride
Similarity: 0.53
[ 832114-00-8 ]
3,5-Dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)isoxazole
Similarity: 0.78
[ 1346808-41-0 ]
5-Methylisoxazole-4-boronic Acid Pinacol Ester
Similarity: 0.69
[ 928664-98-6 ]
4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)isoxazole
Similarity: 0.56