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[ CAS No. 1541-10-2 ] {[proInfo.proName]}

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Chemical Structure| 1541-10-2
Chemical Structure| 1541-10-2
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Product Details of [ 1541-10-2 ]

CAS No. :1541-10-2 MDL No. :MFCD00218475
Formula : C9H12S Boiling Point : -
Linear Structure Formula :- InChI Key :PKANQZUPJCMBAK-UHFFFAOYSA-N
M.W : 152.26 Pubchem ID :284449
Synonyms :

Safety of [ 1541-10-2 ]

Signal Word:Danger Class:9
Precautionary Statements:P261-P305+P351+P338-P342+P311-P273 UN#:3334
Hazard Statements:H319-H334-H410 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 1541-10-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1541-10-2 ]

[ 1541-10-2 ] Synthesis Path-Downstream   1~5

  • 1
  • (2,4,6-trimethylphenylthiolato)(2,2,2-κ3-hydridotris(3-phenyl-5-dimethylpyrazolyl)borate)nickel(II) [ No CAS ]
  • [ 74-88-4 ]
  • [ 1541-10-2 ]
  • [ 7570-91-4 ]
  • [ 3347-62-4 ]
  • 2
  • (2,4,6-trimethylphenylthiolato)(2,2,2-κ3-hydridotris(3-phenyl-5-dimethylpyrazolyl)borate)nickel(II) [ No CAS ]
  • [ 107-06-2 ]
  • [ 1541-10-2 ]
  • [ 1483-92-7 ]
  • C10H13ClS [ No CAS ]
  • [ 3347-62-4 ]
  • 3
  • [ 1541-10-2 ]
  • [ 171408-84-7 ]
  • C43H36O4S2 [ No CAS ]
  • 4
  • [ 1541-10-2 ]
  • [ 171408-84-7 ]
  • 2,7-bis(mesitylthio)-9,9′-spirobifluorene [ No CAS ]
  • 5
  • [ 1541-10-2 ]
  • [ 1835-65-0 ]
  • C17H11F3N2S [ No CAS ]
YieldReaction ConditionsOperation in experiment
68.1% With potassium fluoride; In acetonitrile; at 5 - 20℃; for 3h; General procedure: In the synthesis of Example 1 (1) The compound (4-1), except that a beta-naphthol(compound (a-1)), a 2,4,6-trimethyl-thiophenol (Compound (a-2)) It is to obtain a compound (4-2) in the same manner (yield: 68.1percent).
3.7 g With potassium fluoride; In acetonitrile; at 20 - 25℃; for 2h; Thetetrafluoro Phthalo nitrile (compound (5)) 3.0 g (15mmol), and the potassiumfluoride 15 g (1.2eq.) and acetonitrile 20ml were put in the reactor in whichthe entrance of 100ml placing the thermometer was 4 and it was stirred and itcooled to 5. Here, 2, 4, 6- trimethyl thiophenol (compound(a-11): purity 77percent) 3.0 g (1.0eq.) was unloaded. The temperature of the mixturewas increased to 20 and it reacted at 20 through25 after the load finish. Thereaction mixture was emitted to water after the completion of reaction and thesegregatedsolid was filtered and it took out. The obtained crude product was well wipedoff with the isopropanol and it dried and the compound (4-1) 3.7g which was thewhite solid was obtained (yield 74percent).
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