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[ CAS No. 14916-87-1 ] {[proInfo.proName]}

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Chemical Structure| 14916-87-1
Chemical Structure| 14916-87-1
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Product Details of [ 14916-87-1 ]

CAS No. :14916-87-1 MDL No. :MFCD00274642
Formula : C32CuF16N8 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 863.92 Pubchem ID :-
Synonyms :

Safety of [ 14916-87-1 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 14916-87-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 14916-87-1 ]

[ 14916-87-1 ] Synthesis Path-Downstream   1~8

  • 1
  • [ 1835-65-0 ]
  • copper(l) chloride [ No CAS ]
  • [ 14916-87-1 ]
  • 2
  • [ 1835-65-0 ]
  • [ 12775-96-1 ]
  • [ 14916-87-1 ]
  • 3
  • [ 1835-65-0 ]
  • copper dichloride [ No CAS ]
  • [ 14916-87-1 ]
  • 4
  • [ 1835-65-0 ]
  • [ 142-71-2 ]
  • [ 14916-87-1 ]
  • 5
  • [ 1835-65-0 ]
  • [ 14916-87-1 ]
  • 6
  • [ 1835-65-0 ]
  • copper(l) chloride [ No CAS ]
  • [ 218598-82-4 ]
  • [ 14916-87-1 ]
  • [ 955131-06-3 ]
YieldReaction ConditionsOperation in experiment
In 1-methyl-pyrrolidin-2-one; at 180℃; for 3h;Inert atmosphere; Synthesis of Exemplified Compounds (P-1-1), (P-2-1), and (P-3-1)Under nitrogen atmosphere, in 50 ml of 1-methyl-2-pyrrolidone, were dissolved 3.0 g (15 mmol) of <strong>[1835-65-0]tetrafluorophthalonitrile</strong>, 1.5 g (5.0 mmol) of synthesis intermediate (B), and 0.99 g (10 mmol) of copper chloride (I), and then stirred for 3 hours at 180° C. After cooling the reaction mixture to room temperature, it was poured into 200 ml of a 5percent hydrochloric acid. Consequently, blue crystals were precipitated. These crystals were separated by a filtration under reduced pressure, followed by washing with water and then acetonitrile, and thereafter drying. Further, they were boiled with 50 ml of acetonitrile for 1 hour, and allowed to cool down to room temperature. The resultant precipitates were separated by a filtration under reduced pressure, and then dried. Thereby was obtained 2.2 g (Yield: 45percent) of a mixture (PP-1) (Melting point>200° C.) containing the exemplified compounds (P-1-1), (P-2-1), and (P-3-1) of the present invention; and hexadecafluoro cupper phthalocyanine (F16CuPc).A mixing rate of phthalocyanine derivatives was measured by a liquid chromatography mass spectrometric analysis (LCMS). The result in terms of area ratio was as follows: (P-1-1):(P-2-1):(P-3-1):(F16CuPc)=54.0:26.4:4.1:15.5 (Since a molar absorption intensity of each of (P-1-1), (P-2-1), (P-3-1), and (F16CuPc) at a detecting wavelength of 254 nm is almost same, the ratio measured from the area results in equal to a molar ratio.).Measuring conditions: TSK gel ODS-80Ts (2 mm Phi.x.150 mm), elute: a mixed solution of A/B (volume ratio 3:7) from 0 minute to 15 minutes, and a mixed solution of A/B (volume ratio 15:85) from 15 minutes to 20 minutes) (elute A: water, elute B: a mixed solution of tetrahydrofuran/methanol (volume ratio 9:1)), flow rate: 0.2 ml/min, a detecting wavelength 254 nm, structural determination by atmospheric pressure chemical ionization (APCI)-mass spectrometry (MS) (It was confirmed using MS that a peak at the retention time=8.185 minutes was (F16CuPc), a peak at the retention time=11.676 minutes was (P-1-1), a peak at the retention time=13.905 minutes was (P-2-1), and a peak at the retention time=14.350 minutes was (P-3-1)). A peak was detected in the blank at the retention time of from 0 to 4 minutes, so that a measurement was started from 4 minutes.
  • 8
  • [ 1835-65-0 ]
  • copper(l) chloride [ No CAS ]
  • [ 14916-87-1 ]
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