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[ CAS No. 14516-54-2 ] {[proInfo.proName]}

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Chemical Structure| 14516-54-2
Chemical Structure| 14516-54-2
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Product Citations

Product Citations

Valdivieso, Jorge P ; Erickson, Alexander N ; Gardinier, James R DOI: PubMed ID:

Abstract: A series of rhenium and complexes of a heteroscorpionate ligand with an atypical N2P-donor set has been prepared to better understand their electronic and CO releasing properties. Thus, the ligand, pz2TTP, with an a,a-bis(pyrazol-1-yl)tolyl group decorated with an ortho-situated di(ptolyl)phosphanyl reacts with carbonyl group 17 reagents to give [fac-(k2 NP-pz2TTP)Re(CO)3Br], 1, and [fac-(k3 N2P-pz2TTP)M(CO)3](OTf = O3SCF3), 2-M (M = Re, Mn), if care is taken during the preparation of the manganeses derivative. When heated in CH3CN, 2-Mn slowly transforms to [fac,cis-(k3 N2P-pz2TTP) Mn(CO)2(NCCH3)](OTf), 3-Mn. In contrast, the corresponding 3-Re can only be prepared from 2-Re using Me3NO; pure 3-Mn can also be prepared by this method. Experimental and density functional calculations at the M06L/Def2-TZVP/PCM(CH3CN) level show that the replacement of a carbonyl with an acetonitrile solvent decreases the oxidation potential by around 0.8 V per carbonyl released, making decarbonylated species potent reductants. At the same time, the electronic spectrum broadens and undergoes a red-shift, making dicarbonyl complexes more susceptible to photo-initiated decarbonylation reactions than tricarbonyls. When 2-Mn or 3-Mn are irradiated in with 390 nm LED light in aerated solutions, [trans-Mn(pz2TTP = O)2](OTf)2, 4, along with insoluble manganese oxides are rapidly formed.

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Product Details of [ 14516-54-2 ]

CAS No. :14516-54-2 MDL No. :MFCD00049806
Formula : C5BrMnO5 Boiling Point : -
Linear Structure Formula :- InChI Key :LOCZKKJCQVRJPQ-UHFFFAOYSA-M
M.W : 274.89 Pubchem ID :10978692
Synonyms :

Safety of [ 14516-54-2 ]

Signal Word:Danger Class:6.1
Precautionary Statements:P261-P264-P270-P271-P280-P302+P352-P304+P340-P312-P330-P363-P403-P501 UN#:3466
Hazard Statements:H301-H311-H331 Packing Group:Ⅲ
GHS Pictogram:

Application In Synthesis of [ 14516-54-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 14516-54-2 ]

[ 14516-54-2 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 14516-54-2 ]
  • [ 1088-00-2 ]
  • [ 385815-53-2 ]
  • 2
  • [ 97239-80-0 ]
  • [ 14516-54-2 ]
  • [ 1380506-78-4 ]
  • 3
  • [ 14516-54-2 ]
  • [ 17217-57-1 ]
  • Mn(4,4'-dimethoxy-2,2′-bipyridine)(CO)<SUB>3</SUB>Br [ No CAS ]
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