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Chemical Structure| 144-48-9 Chemical Structure| 144-48-9
Chemical Structure| 144-48-9

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CAS No.: 144-48-9

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2-Iodoacetamide is a commonly used alkylating agent, primarily employed for cysteine alkylation in proteomics, aiding in detailed protein analysis and research.

Synonyms: Iodoacetamide; IA; IAM

4.5 *For Research Use Only !

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Product Details of 2-Iodoacetamide

CAS No. :144-48-9
Formula : C2H4INO
M.W : 184.96
SMILES Code : NC(=O)CI
Synonyms :
Iodoacetamide; IA; IAM
MDL No. :MFCD00008028
InChI Key :PGLTVOMIXTUURA-UHFFFAOYSA-N
Pubchem ID :3727

Safety of 2-Iodoacetamide

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H301-H317-H334
Precautionary Statements:P261-P280-P301+P310-P342+P311
Class:6.1
UN#:2811
Packing Group:Ⅲ

Application In Synthesis of 2-Iodoacetamide

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 144-48-9 ]

[ 144-48-9 ] Synthesis Path-Downstream   1~5

  • 1
  • [ 144-48-9 ]
  • [ 101-06-4 ]
  • [ 137089-44-2 ]
  • 2
  • [ 144-48-9 ]
  • [ 107-18-6 ]
  • [ 10374-51-3 ]
  • 3
  • [ 2166-13-4 ]
  • [ 144-48-9 ]
  • [ 86894-59-9 ]
  • 4
  • [ 144-48-9 ]
  • [ 18362-30-6 ]
  • [ 1000267-52-6 ]
YieldReaction ConditionsOperation in experiment
90% 1.0 g of 6-chlorosalicylaldehyde 9 is dissolved in 30 ml of DMF, 0.26 g of NaH (60percent suspension in paraffin oil) is carefully added with cooling, and the mixture is stirred at RT for 45 min. 1.30 g of 2-iodoacetamide 2 are then added, and the reaction mixture is stirred overnight. The mixture is subsequently subjected to conventional work-up, giving 1.28 g (90percent) of 2-(3-chloro-2-formylphenoxy)acetamide 10 ; MS-EI (M+)=213
  • 5
  • [ 144-48-9 ]
  • [ 97817-23-7 ]
  • 2-(2-amino-6,7-dihydro[1,3]thiazolo[5,4-c]pyridin-5(4H)-yl)acetamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
54% With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20℃; To a mixture of <strong>[97817-23-7]4,5,6,7-tetrahydro[1,3]thiazolo[5,4-c]pyridin-2-amine</strong> (50 mg, 0.322 mmol) and DIPEA (0.072 mL, 0.418 mmol) in THE (3 mL), 2-iodoacetamide (65 mg, 0.354 mmol) was added and the reaction let under stirring at rt overnight. After solvent removal under reduced pressure, the title compound was isolated by column chromatography (eluant DCM:MeOH = 90:10) as white solid (37 mg, 54%).NMR (500 MHz, DMSO-d6) ppm 2.73 (t, J=5.72 Hz, 2 H) 3.03 (s, 2 H) 3.46 (s, 2 H) 6.70 (br. s., 2 H) 7.12 (br. s.,H) 7.23 (br. s., 1 H).HRMS (ESI+): calcd. for 08H13N40S [M + H] 213.0805; found 213.0799.
 

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