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CAS No. : | 142733-64-0 | MDL No. : | MFCD08436074 |
Formula : | C10H19NO3 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | PCPNTJQMXAHNOA-UHFFFAOYSA-N |
M.W : | 201.26 | Pubchem ID : | 22408683 |
Synonyms : |
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Chemical Name : | tert-Butyl (cis-3-(hydroxymethyl)cyclobutyl)carbamate |
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P280-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With hydrogenchloride; In 1,4-dioxane; dichloromethane; at 20.0℃; | To a solution of tert-butyl (cis-3-(hydroxymethyl)cyclobutyl)carbamate (0.154 g, 0.765 mmol) in DCM (2 mL), HC1 4N in dioxane (0.4 mL, 1.6 mmol) was added at rt. After 5h30 min a further aliquot of HC1 4N in dioxane (0.8 mL, 3.2 mmol) was added and mixture was left at rt until complete conversion. Mixture was evaporated under reduced pressure to obtain cis- 3- (hydroxymethyl)cyclobutan-l-aminium chloride as a white solid (128 mg). Method 1 : Rt=0.83 min, m/z=l02 (M+H)+. The crude compound (38.5 mg, 0.280 mmol) was taken in dry acetonitrile (1.7 mL) and dry DIPEA (0.1 mL, 0.574 mmol) and ethyl 4-(chlorosulfonyl)-3-fluoro-l-methyl- lH-pyrrole-2-carboxylate (50 mg, 0.185 mmol) were added at room temperature. Reaction mixture was stirred overnight and then evaporated under reduced pressure to afford a light brown solid. Crude was purified with flash chromatography (Petroleum ether/ AcOEt) to afford D42 as a white solid (45 mg) m/z = 335 (M+H)+. |