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Chemical Structure| 14099-01-5 Chemical Structure| 14099-01-5

Structure of 14099-01-5

Chemical Structure| 14099-01-5

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CAS No.: 14099-01-5

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Product Details of [ 14099-01-5 ]

CAS No. :14099-01-5
Formula : C5ClO5Re
M.W : 361.71
SMILES Code : [C]=O.[C]=O.[C]=O.[C]=O.[C]=O.[Re]Cl
MDL No. :MFCD00013296
InChI Key :JQUUAHKBIXPQAP-UHFFFAOYSA-M
Pubchem ID :6096982

Safety of [ 14099-01-5 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H301+H311+H331-H315-H319-H335
Precautionary Statements:P261-P280-P302+P352+P312-P304+P340+P312-P403+P233
Class:6.1
UN#:3288
Packing Group:Ⅲ

Application In Synthesis of [ 14099-01-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 14099-01-5 ]

[ 14099-01-5 ] Synthesis Path-Downstream   1~24

  • 1
  • [ 14099-01-5 ]
  • [ 17217-57-1 ]
  • [ 134438-70-3 ]
  • 2
  • [ 14099-01-5 ]
  • [ 66127-01-3 ]
  • fac-ReCl(CO)3(3-bromophenathroline) [ No CAS ]
  • 3
  • [ 14099-01-5 ]
  • [ 2923-28-6 ]
  • [ 112881-51-3 ]
  • [ 75-05-8 ]
  • [ 515125-23-2 ]
  • 4
  • [ 387-97-3 ]
  • [ 14099-01-5 ]
  • [ 108-88-3 ]
  • [fac-Re(5-fluoro-8-hydroxyquinolate)(CO)3]2 [ No CAS ]
  • [fac-Re(5-fluoro-8-quinolate)(CO)3](μ-Cl)[fac-Re(5-fluoro-8-quinoline)(CO)3]*toluene [ No CAS ]
  • 5
  • [ 387-97-3 ]
  • [ 14099-01-5 ]
  • [fac-Re(5-fluoro-8-hydroxyquinolate)(CO)3]2 [ No CAS ]
  • 6
  • [ 33893-89-9 ]
  • [ 14099-01-5 ]
  • [ 1440544-05-7 ]
  • 7
  • [ 14099-01-5 ]
  • [ 81998-05-2 ]
  • [ 1446281-30-6 ]
  • 8
  • [ 14099-01-5 ]
  • [ 4591-55-3 ]
  • fac-rhenium tricarbonyl bis(dimethyl pyridine-3,5-dicarboxylate) chloride [ No CAS ]
  • 9
  • [ 5394-23-0 ]
  • [ 14099-01-5 ]
  • fac-[ReCl(4,7-dichloro-1,10-phenanthroline)(CO)3] [ No CAS ]
  • 10
  • [ 14099-01-5 ]
  • [ 7089-68-1 ]
  • (2-chloro-1,10-phenanthroline)rhenium(I) [ No CAS ]
  • 11
  • [ 14099-01-5 ]
  • [ 17217-57-1 ]
  • [ 134438-70-3 ]
  • 12
  • [ 14099-01-5 ]
  • [ 14173-30-9 ]
  • C9H7ClNO5Re [ No CAS ]
YieldReaction ConditionsOperation in experiment
56% In ethanol; for 3h;Heating; A mass of 97 mg of Hhhp·HCl (552 μmol) was added to a suspension of 100 mg of [Re(CO)5Cl] (276 μmol) in 25 cm3 of ethanol. After heating of the mixture for 3 h, the solution was cooled to room temperature and filtered. The filtrate was left to evaporate at room temperature, and after 5 days yellow crystals, suitable for X-ray diffraction studies, were collected by filtration. They were washed with acetone and diethyl ether, and dried under vacuum. Yield = 67 mg (56%), m.p. = 169 C. Anal. Calc. for C9H7ClNO5Re:C, 25.1; H, 1.6; N, 3.3. Found: C, 25.3;H, 1.4; N, 3.7%. IR (νmax cm-1): ν(C≡O(shè)) 1881vs, 2023vs; ν(Re-N) 486m; ν(Re-O) 431m; ν(O-H) 3270m. 1H NMR (295 K, ppm): 8.41 (d, 1H, H(15)), 7.55 (t, 1H, H(14)),7.68 (d,1H, H(13)), 2.49 (s, 2H, H(1)), 3.45 (s, 1H, O(1)H). Conductivity (10-3 M, DMF): 17.
  • 13
  • [ 14099-01-5 ]
  • [ 131747-63-2 ]
  • [ 99-98-9 ]
  • C17H14BrClN3O3Re [ No CAS ]
  • 14
  • [ 14099-01-5 ]
  • [ 131747-63-2 ]
  • [ 62-53-3 ]
  • C15H9BrClN2O3Re [ No CAS ]
  • 15
  • [ 14099-01-5 ]
  • [ 131747-63-2 ]
  • [ 87-62-7 ]
  • C17H13BrClN2O3Re [ No CAS ]
  • 16
  • [ 14099-01-5 ]
  • [ 131747-63-2 ]
  • [ 95-51-2 ]
  • C15H8BrCl2N2O3Re [ No CAS ]
  • 17
  • [ 14099-01-5 ]
  • [ 131747-63-2 ]
  • [ 106-49-0 ]
  • C16H11BrClN2O3Re [ No CAS ]
  • 18
  • [ 14099-01-5 ]
  • [ 131747-63-2 ]
  • [ 371-40-4 ]
  • C15H8BrClFN2O3Re [ No CAS ]
  • 19
  • [ 14099-01-5 ]
  • [ 131747-63-2 ]
  • [ 106-47-8 ]
  • C15H8BrCl2N2O3Re [ No CAS ]
  • 20
  • [ 14099-01-5 ]
  • [ 131747-63-2 ]
  • [ 106-40-1 ]
  • C15H8Br2ClN2O3Re [ No CAS ]
  • 21
  • [ 14099-01-5 ]
  • [ 131747-63-2 ]
  • [ 540-37-4 ]
  • C15H8BrClIN2O3Re [ No CAS ]
  • 22
  • [ 14099-01-5 ]
  • [ 455-14-1 ]
  • [ 131747-63-2 ]
  • C16H8BrClF3N2O3Re [ No CAS ]
  • 23
  • [ 14099-01-5 ]
  • [ 13040-77-2 ]
  • tricarbonylchloro(6-chloro-2,2'-bipyridine)rhenium(I) [ No CAS ]
  • 24
  • [ 14099-01-5 ]
  • [ 865169-07-9 ]
  • [Re(CO)3(2-(4-carboxyphenyl)-1H-imidazo[4,5-f][1,10]phenanthroline)Cl] [ No CAS ]
 

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