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Chemical Structure| 1391728-13-4 Chemical Structure| 1391728-13-4
Chemical Structure| 1391728-13-4

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CAS No.: 1391728-13-4

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Product Details of [ 1391728-13-4 ]

CAS No. :1391728-13-4
Formula : C9H10FIO
M.W : 280.08
SMILES Code : CC1(C)OI(F)C2=CC=CC=C12
MDL No. :MFCD28397076
InChI Key :FISITPXJYDTLHI-UHFFFAOYSA-N
Pubchem ID :72546672

Safety of [ 1391728-13-4 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H272
Precautionary Statements:P210-P220-P221-P280-P370+P378-P501
Class:5.1
UN#:1479
Packing Group:Ⅱ

Application In Synthesis of [ 1391728-13-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1391728-13-4 ]

[ 1391728-13-4 ] Synthesis Path-Downstream   1~29

  • 1
  • [ 610-97-9 ]
  • [ 1391728-13-4 ]
  • 2
  • [ 69352-05-2 ]
  • [ 1391728-13-4 ]
YieldReaction ConditionsOperation in experiment
89% With silver(II) fluoride; In acetonitrile; at 20℃; for 1h;Inert atmosphere; General procedure: Under Ar atmosphere, corresponding aryl-iodides (1.0 mmol, 1.0 equiv) and AgF2 (3.3 equiv for 1; 2.5 equiv for 2) and 10 mL anhydrous MeCN were added to a 25mL rounded bottom, then the reaction mixture was allowed to stir at room temperature for 1 hour. The mixture was concentrated under vacuum. Then 20 mL anhydrous ether was added to make desired products dissolve. The mixture was filtered, and the filter cake was washed with a small amount of ether. The combined filtrate was concentrated to afford the desired product 1a-g and 2a-g in 75-95% yield
  • 3
  • [ 69352-04-1 ]
  • [ 1391728-13-4 ]
  • 4
  • [ 1391728-13-4 ]
  • [ 887144-97-0 ]
  • 5
  • [ 134-20-3 ]
  • [ 1391728-13-4 ]
  • 6
  • [ 69352-03-0 ]
  • [ 1391728-13-4 ]
  • 7
  • [ 69429-70-5 ]
  • [ 1391728-13-4 ]
  • 8
  • [ 1459128-72-3 ]
  • [ 1391728-13-4 ]
  • 9
  • [ 1459128-73-4 ]
  • [ 1391728-13-4 ]
  • 10
  • [ 2712-78-9 ]
  • [ 1391728-13-4 ]
  • 11
  • [ 73602-61-6 ]
  • [ 69429-70-5 ]
  • [ 1391728-13-4 ]
  • 12
  • [ 1459128-72-3 ]
  • [ 73602-61-6 ]
  • [ 1391728-13-4 ]
  • 13
  • [ 1459128-73-4 ]
  • [ 73602-61-6 ]
  • [ 1391728-13-4 ]
  • 14
  • [ 1391728-13-4 ]
  • [ 94-02-0 ]
  • C20H21IO4 [ No CAS ]
  • 15
  • [ 1000293-91-3 ]
  • [ 1391728-13-4 ]
  • 3,3-dimethyl-1-(1,1,2,2-tetrafluoro-2-(phenylthio)ethyl)-1,3-dihydro-1λ3-benzo[d][1,2]iodaoxole [ No CAS ]
  • 16
  • [ 1391728-13-4 ]
  • (2-(4-bromophenoxy)-1,1,2,2-tetrafluoroethyl)trimethylsilane [ No CAS ]
  • 1-(2-(4-bromophenoxy)-1,1,2,2-tetrafluoroethyl)-3,3-dimethyl-1,3-dihydro-1λ3-benzo[d][1,2]iodaoxole [ No CAS ]
  • 17
  • [ 1391728-13-4 ]
  • trimethyl(1,1,2,2-tetrafluoro-2-(4-methoxyphenoxy)ethyl)silane [ No CAS ]
  • 3,3-dimethyl-1-(1,1,2,2-tetrafluoro-2-(4-methoxyphenoxy)ethyl)-1,3-dihydro-1λ3-benzo[d][1,2]iodaoxole [ No CAS ]
  • 18
  • [ 1391728-13-4 ]
  • ethyl 4-(1,1,2,2-tetrafluoro-2-(trimethylsilyl)ethoxy)benzoate [ No CAS ]
  • ethyl 4-(2-(3,3-dimethyl-1λ3-benzo[d][1,2]iodaoxol-1(3H)-yl)-1,1,2,2-tetrafluoroethoxy)benzoate [ No CAS ]
  • 19
  • [ 722491-59-0 ]
  • [ 1391728-13-4 ]
  • 1-(2-(3,3-dimethyl-1λ3-benzo[d][1,2]iodaoxol-1(3H)-yl)-1,1,2,2-tetrafluoroethyl)-1H-imidazole [ No CAS ]
YieldReaction ConditionsOperation in experiment
80% With tetrabutylammonium triphenyldifluorosilicate; In acetonitrile; at -35 - 0℃; for 1h; 1 equivalent of 1-[(1,1,2,2-Tetrafluoro-2-trimethylsilyl)ethyl]-lH-imidazole was treated with 2 equivalents of fluoroiodane alcohol in the presence of 1 mol% TBAT in acetonitrile at a temperature of -35C to 0C for 1 hour providing Im-I in 77-80% isolated yield. Similarly as in the case of synthesis of PhS-I, the Um- polung of 1-[(1,1,2,2-Tetrafluoro-2-trimethylsilyl)ethyl]-lH-imidazole with fluoroiodane alcohol was essentially finished within 10 minutes after addition of silane was complete (as evidenced by TLC analysis). Reagent Im-I was obtained as a viscous yellowish liquid that soon crystallized at ambient temperature (20C to 25C) .
  • 20
  • [ 1125518-69-5 ]
  • [ 1391728-13-4 ]
  • 1-(2-(3,3-dimethyl-1λ3-benzo[d][1,2]iodaoxol-1(3H)-yl)-1,1,2,2-tetrafluoroethyl)-1H-benzo[d]imidazole [ No CAS ]
  • 21
  • [ 1125518-71-9 ]
  • [ 1391728-13-4 ]
  • 1-(2-(3,3-dimethyl-1λ3-benzo[d][1,2]iodaoxol-1(3H)-yl)-1,1,2,2-tetrafluoroethyl)-1H-pyrazole [ No CAS ]
  • 22
  • [ 1391728-13-4 ]
  • pyren-1-ylmethyl 3-(2-(1,1,2,2-tetrafluoro-2-(trimethylsilyl)ethoxy)phenyl)propanoate [ No CAS ]
  • pyren-1-ylmethyl 3-(2-(2-(3,3-dimethyl-1λ3-benzo[d][1,2]iodaoxol-1(3H)-yl)-1,1,2,2-tetrafluoroethoxy)phenyl)propanoate [ No CAS ]
  • 23
  • [ 1391728-13-4 ]
  • [ 174708-24-8 ]
  • [ 69352-05-2 ]
  • 6-benzyl-6-fluorotetrahydro-2H-pyran-2-one [ No CAS ]
  • 2-(2-iodophenyl)propan-2-yl 5-oxo-6-phenylhexanoate [ No CAS ]
  • 24
  • [ 1391728-13-4 ]
  • trimethyl(1,1,2,2-tetrafluoro-2-(phenylsulfonyl)ethyl)silane [ No CAS ]
  • C17H15F4IO3S [ No CAS ]
YieldReaction ConditionsOperation in experiment
32% With tetrabutylammonium triphenyldifluorosilicate; In acetonitrile; at -35 - 0℃; for 1h; The reaction of PhSO2CF2CF2TMS with 2 equivalents of fluoroiodane alcohol in the presence of 1 moll TBAT at -35 C in MeCN gave 48% NMR yield of PhSO2-I. Pure PhSC>2-I could be obtained in 32% isolated yield.
  • 25
  • [ 1391728-13-4 ]
  • (2-(2-(1,3-dioxolan-2-yl)phenoxy)-1,1,2,2-tetrafluoroethyl)trimethylsilane [ No CAS ]
  • 1-(2-(2-(1,3-dioxolan-2-yl)phenoxy)-1,1,2,2-tetrafluoroethyl)-3,3-dimethyl-1,3-dihydro-1λ3-benzo[d][1,2]iodaoxole [ No CAS ]
  • 26
  • [ 1391728-13-4 ]
  • methyl 4-(2,2,3,3-tetrafluoro-3-(trimethylsilyl)propyl)benzoate [ No CAS ]
  • methyl 4-(3-(3,3-dimethyl-1λ3-benzo[d][1,2]iodaoxol-1(3H)-yl)-2,2,3,3-tetrafluoropropyl)benzoate [ No CAS ]
  • 27
  • [ 1391728-13-4 ]
  • 4-methyl-7-(1,1,2,2-tetrafluoro-2-(trimethylsilyl)ethoxy)-2H-chromen-2-one [ No CAS ]
  • 7-(2-(3,3-dimethyl-1λ3-benzo[d][1,2]iodaoxol-1(3H)-yl)-1,1,2,2-tetrafluoroethoxy)-4-methyl-2H-chromen-2-one [ No CAS ]
  • 28
  • [ 1391728-13-4 ]
  • 4-methyl-7-((1,1,2,2-tetrafluoro-2-(trimethylsilyl)ethyl)thio)-2H-chromen-2-one [ No CAS ]
  • 7-((2-(3,3-Dimethyl-1λ3-benzo[d][1,2]iodaoxol-1(3H)-yl)-1,1,2,2-tetrafluoroethyl)thio)-4-methyl-2H-chromen-2-one [ No CAS ]
  • 29
  • triethyl(perfluoroethyl)silane [ No CAS ]
  • [ 1391728-13-4 ]
  • 3,3-dimethyl-1-(perfluoroethyl)-1,3-dihydro-1λ3-benzo[d][1,2]iodaoxole [ No CAS ]
 

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