Purity | Size | Price | VIP Price | USA Stock *0-1 Day | Global Stock *5-7 Days | Quantity | ||||||
{[ item.p_purity ]} | {[ item.pr_size ]} | Inquiry |
{[ getRatePrice(item.pr_usd, 1,1,item.pr_is_large_size_no_price) ]} {[ getRatePrice(item.pr_usd,item.pr_rate,1,item.pr_is_large_size_no_price) ]} |
{[ getRatePrice(item.pr_usd, 1,1,item.pr_is_large_size_no_price) ]} | Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price) ]} {[ getRatePrice(item.pr_usd,1,item.mem_rate,item.pr_is_large_size_no_price) ]} | {[ item.pr_usastock ]} | in stock Inquiry - | {[ item.pr_chinastock ]} | {[ item.pr_remark ]} in stock Inquiry - | Login | Inquiry |
Please Login or Create an Account to: See VIP prices and availability
CAS No. : | 124-19-6 | MDL No. : | MFCD00007030 |
Formula : | C9H18O | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | GYHFUZHODSMOHU-UHFFFAOYSA-N |
M.W : | 142.24 | Pubchem ID : | 31289 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P264-P273-P280-P302+P352-P332+P313-P362+P364 | UN#: | N/A |
Hazard Statements: | H315-H412 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
58% | General procedure: A dry and argon-flushed round bottom flask equipped with a magnetic stirrer and a septum was charged with a solution of 3 or 5 (1 equiv.) in dry THF (20 mL) and was cooled at -78 C. A solution of iPrMgCl·LiCl (1.3 equiv.) was added dropwise and the reaction mixture was stirred for 30 minutes at -78 C. The corresponding aldehyde was added and the reaction mixture was slowly warmed to room temperature and stirred overnight. The reaction mixture was hydrolysed with water (20 mL) and extracted with EtOAc (3 × 20 mL). The combined organic layers were washed with brine (20 mL), dried over MgSO4, and concentrated under reduced pressure. The residue was purified by column chromatography on silica gel. |