Purity | Size | Price | VIP Price | USA Stock *0-1 Day | Global Stock *5-7 Days | Quantity | ||||||
{[ item.p_purity ]} | {[ item.pr_size ]} | Inquiry |
{[ getRatePrice(item.pr_usd, 1,1,item.pr_is_large_size_no_price) ]} {[ getRatePrice(item.pr_usd,item.pr_rate,1,item.pr_is_large_size_no_price) ]} |
{[ getRatePrice(item.pr_usd, 1,1,item.pr_is_large_size_no_price) ]} | Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price) ]} {[ getRatePrice(item.pr_usd,1,item.mem_rate,item.pr_is_large_size_no_price) ]} | {[ item.pr_usastock ]} | in stock Inquiry - | {[ item.pr_chinastock ]} | {[ item.pr_remark ]} in stock Inquiry - | Login | Inquiry |
Please Login or Create an Account to: See VIP prices and availability
CAS No. : | 1190360-23-6 | MDL No. : | MFCD28955974 |
Formula : | C15H13Br | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | VECLPBKDHAALGQ-UHFFFAOYSA-N |
M.W : | 273.17 | Pubchem ID : | 59629661 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302-H315-H319 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
50 mmol | Step1. Dissolve 100 mmol of 3-bromo-9,9-dimethylfluorene in anhydrous THF and cool to - 78 C, argon.Under the protection of gas, 1.5 equivalents of n-butyllithium was added and reacted for 1 h. The temperature was slowly raised to room temperature, triphenylgermanium chloridewas added, and the reaction was completed in 1 h. The reaction was quenched with EtOAc EtOAc.The silica gel column was passed to give the product 37 50 mmol. |