成人免费xx,国产又黄又湿又刺激不卡网站,成人性视频app菠萝网站,色天天天天

Home Cart 0 Sign in  

[ CAS No. 113283-93-5 ] {[proInfo.proName]}

,{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]}
Chemical Structure| 113283-93-5
Chemical Structure| 113283-93-5
Structure of 113283-93-5 * Storage: {[proInfo.prStorage]}

Please Login or Create an Account to: See VIP prices and availability

Cart0 Add to My Favorites Add to My Favorites Bulk Inquiry Inquiry Add To Cart

Search after Editing

* Storage: {[proInfo.prStorage]}

* Shipping: {[proInfo.prShipping]}

Quality Control of [ 113283-93-5 ]

Related Doc. of [ 113283-93-5 ]

Alternatived Products of [ 113283-93-5 ]
Product Citations

Product Details of [ 113283-93-5 ]

CAS No. :113283-93-5 MDL No. :MFCD08729301
Formula : C9H20N2O2 Boiling Point : No data available
Linear Structure Formula :- InChI Key :JMIGZQVLLZKDIS-UHFFFAOYSA-N
M.W : 188.27 Pubchem ID :13855174
Synonyms :

Safety of [ 113283-93-5 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P305+P351+P338 UN#:
Hazard Statements:H302-H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 113283-93-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 113283-93-5 ]

[ 113283-93-5 ] Synthesis Path-Downstream   1~14

  • 1
  • [ 110-72-5 ]
  • [ 24424-99-5 ]
  • [ 113283-93-5 ]
YieldReaction ConditionsOperation in experiment
Reference Example 15 N-(2-aminoethyl)-N-ethyl-2,2,2-trifluoroacetamide hydrochloride According to the method described in Synthetic Communications, 23(17), 2443-2449 (1993), tert-butyl N-[2-(ethylamino)ethyl]carbamate (3.06 g, 16.25 mmol) was obtained from N-ethylethylenediamine (8.36 g) and di-tert-butyl dicarbonate (6.25 g).
3.2 g In tetrahydrofuran; at 0 - 20℃; In a round bottom flask, N-ethylethylenediamine (8.82 g) was dissolved in 200 ml of anhydrous THF, the solution was cooled to 0-5 C. and di-tert-butyl dicarbonate (6.54 g) dissolved in 60 ml of THF was added during one hour. The mixture was stirred overnight at room temperature. Next, the solvent was distilled off, the residue was dissolved in saturated NaCl solution (60 ml) and the product was extracted with dichloromethane (3*60 ml). The extract was washed with a saturated NaCl solution (60 ml) and dried with anhydrous MgSO4. Next, the solvent was distilled off under reduced pressure and the obtained product was recrystallized from hexane giving 3.2 g of the desired product.
  • 2
  • [ 31139-36-3 ]
  • [ 113283-93-5 ]
  • [ 113283-95-7 ]
  • 3
  • [ 113283-91-3 ]
  • [ 113283-93-5 ]
  • 4
  • [ 98-88-4 ]
  • [ 113283-93-5 ]
  • [2-(Benzoyl-ethyl-amino)-ethyl]-carbamic acid tert-butyl ester [ No CAS ]
  • 5
  • [ 113283-93-5 ]
  • [ 98-59-9 ]
  • [ 135250-93-0 ]
  • 6
  • [ 110-72-5 ]
  • [ 13139-12-3 ]
  • [ 113283-93-5 ]
  • 7
  • [ 113283-93-5 ]
  • 3-iodo-6-(2-methoxyphenyl)-5-methylpyridazine [ No CAS ]
  • N-1-ethyl-N-1-[6-(2-methoxy-phenyl)-5-methyl-pyridazin-3-yl]-ethane-1,2-diamine [ No CAS ]
  • 8
  • [ 113283-93-5 ]
  • [ 4457-32-3 ]
  • N-(tert-butoxycarbonyl)-2-[ethyl(4-nitrobenzyloxycarbonyl)amino]ethylamine [ No CAS ]
  • 10
  • [ 110-72-5 ]
  • CaH [ No CAS ]
  • [ 24424-99-5 ]
  • [ 113283-93-5 ]
YieldReaction ConditionsOperation in experiment
With sodium chloride; In tetrahydrofuran; Step 1. Synthesis of (2-ethylaminoethylearbamic acid, 1,1-dimethylethyl ester) (3) Refer to . A 25 g (0.28 mol) quantity of N-ethylethylenediamine (1) was placed in a dried 500 ml rb flask. THF, 250 ml, previously dried by distillation from CaH, was added via cannula. The flask was kept under argon and cooled in an ice bath for 20 minutes. A dried addition funnel was charged with 50 ml THF to which was added 29.3 ml (0.13 mol) of di-tert-butyl dicarbonate (2). This mixture was added slowly dropwise to the stirred amine. After addition was complete, the reaction was removed from the ice bath and allowed to stir and reach ambient temperature overnight. The volatiles were removed by rotary evaporation. Saturated NaCl (50 ml) was added, and the result extracted with 4*100 ml ethyl acetate. The combined organic fractions were dried over Na2SO4 overnight. The drying agent was removed by filtration and the volatiles removed by rotary evaporation to yield 2-ethylaminoethylcarbamic acid, 1,1 -dimethylethyl ester (3; 27.55 g, 0.15 mol). The material was used without further purification.
  • 11
  • [ 39684-80-5 ]
  • [ 75-04-7 ]
  • [ 113283-93-5 ]
  • 12
  • [ 1203701-93-2 ]
  • [ 113283-93-5 ]
  • [ 1203701-96-5 ]
  • 13
  • [ 89711-08-0 ]
  • [ 75-04-7 ]
  • [ 113283-93-5 ]
YieldReaction ConditionsOperation in experiment
A solution of the aldehyde A1IJl g, 18.85 mmol) in MeOH (20 ml) was treated with ethylamine (10.37 ml, 20.73 mmol) and stirred at RT for 5 min. The mixture was treated with sodium borohydride (0.856 g, 22.62 mmol). After stirring for 5 min, the mixture was quenched with water and concentrated. The residue was diluted with water, saturated with NaCl, and extracted twice with THF. The organic phase was dried over Na2SO4, filtered and concentrated to yield A-2 as a colorless cloudy oil.
  • 14
  • [ 1104546-96-4 ]
  • [ 113283-93-5 ]
  • [ 1104546-97-5 ]
YieldReaction ConditionsOperation in experiment
With triethylamine; In tetrahydrofuran; at 20℃; for 0.75h; A solution of the amine A1I (425 mg, 2.256 mmol) and TEA (0.629 ml, 4.51 mmol) in THF (10 ml) was treated slowly with acid chloride (500 mg, 2.256 mmol) and stirred at RT for 45 min. The mixture was diluted with EtOAc and was washed with water and brine. The organic phase was dried over Na2SO4, filtered and concentrated. The crude material was purified by gradient elution on silica gel (0 to 55% EtOAc in Hex) to yield A-4 as a colorless film. Data for AA: LRMS m/z (M+H): 374.01
Recommend Products
Same Skeleton Products

Technical Information

Historical Records

Related Functional Groups of
[ 113283-93-5 ]

Aliphatic Chain Hydrocarbons

Chemical Structure| 117499-16-8

[ 117499-16-8 ]

Di-tert-butyl (azanediylbis(ethane-2,1-diyl))dicarbamate

Similarity: 1.00

Chemical Structure| 122734-32-1

[ 122734-32-1 ]

tert-Butyl (2-(methylamino)ethyl)carbamate

Similarity: 0.97

Chemical Structure| 79513-35-2

[ 79513-35-2 ]

tert-Butyl (2-aminoethyl)carbamate hydrochloride

Similarity: 0.95

Chemical Structure| 38267-76-4

[ 38267-76-4 ]

tert-Butyl ethylcarbamate

Similarity: 0.92

Chemical Structure| 100927-10-4

[ 100927-10-4 ]

(R)-tert-Butyl (1-aminopropan-2-yl)carbamate

Similarity: 0.90

Amides

Chemical Structure| 117499-16-8

[ 117499-16-8 ]

Di-tert-butyl (azanediylbis(ethane-2,1-diyl))dicarbamate

Similarity: 1.00

Chemical Structure| 122734-32-1

[ 122734-32-1 ]

tert-Butyl (2-(methylamino)ethyl)carbamate

Similarity: 0.97

Chemical Structure| 79513-35-2

[ 79513-35-2 ]

tert-Butyl (2-aminoethyl)carbamate hydrochloride

Similarity: 0.95

Chemical Structure| 140447-78-5

[ 140447-78-5 ]

1-(2-N-Boc-Aminoethyl)piperazine

Similarity: 0.92

Chemical Structure| 38267-76-4

[ 38267-76-4 ]

tert-Butyl ethylcarbamate

Similarity: 0.92

Amines

Chemical Structure| 117499-16-8

[ 117499-16-8 ]

Di-tert-butyl (azanediylbis(ethane-2,1-diyl))dicarbamate

Similarity: 1.00

Chemical Structure| 122734-32-1

[ 122734-32-1 ]

tert-Butyl (2-(methylamino)ethyl)carbamate

Similarity: 0.97

Chemical Structure| 79513-35-2

[ 79513-35-2 ]

tert-Butyl (2-aminoethyl)carbamate hydrochloride

Similarity: 0.95

Chemical Structure| 140447-78-5

[ 140447-78-5 ]

1-(2-N-Boc-Aminoethyl)piperazine

Similarity: 0.92

Chemical Structure| 38267-76-4

[ 38267-76-4 ]

tert-Butyl ethylcarbamate

Similarity: 0.92

; ;