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CAS No. : | 110-30-5 | MDL No. : | MFCD00059224 |
Formula : | C38H76N2O2 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | RKISUIUJZGSLEV-UHFFFAOYSA-N |
M.W : | 593.02 | Pubchem ID : | 8044 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
94.3% | Stage #1: at 100℃; for 0.166667 h; Inert atmosphere Stage #2: for 6 h; Inert atmosphere |
stearic acid 0.28percent of the composite antioxidant was added to the reaction kettle, and the mixture was slowly heated to 100 ° C after stirring for N2 and 10 min. The stearic acid was completely melted and the 0.20percent composite catalyst with the weight of ethylenediamine and stearic acid was added. Constant temperature reaction for 2 hours, And then slowly heated to 180 ° C, constant temperature reaction for 4 hours to dehydration reaction,The water generated during the reaction is taken out of N2 to stop the reaction, Cooled to 160 ° C discharge.Wherein the molar ratio of stearic acid to ethylenediamine is 1: 0.58; the antioxidant 1076 in the antioxidant,The ratio of the antioxidant DLTDP to the antioxidant T501 was 0.20: 0.36: 1; the composite catalyst was prepared by using the p-toluenesulfonic acid / SAPO-34 supported solid acid catalyst prepared in Example 1 and Example 2 and the phosphoric acid / SiO2-Al2O3 supported solid acid catalyst, the mass ratio of 1: 3.5. The yield of N,N'-ethylenebis(stearamide) |
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