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Chemical Structure| 110-30-5 Chemical Structure| 110-30-5
Chemical Structure| 110-30-5

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CAS No.: 110-30-5

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Product Details of [ 110-30-5 ]

CAS No. :110-30-5
Formula : C38H76N2O2
M.W : 593.02
SMILES Code : CCCCCCCCCCCCCCCCCC(NCCNC(CCCCCCCCCCCCCCCCC)=O)=O
MDL No. :MFCD00059224
InChI Key :RKISUIUJZGSLEV-UHFFFAOYSA-N
Pubchem ID :8044

Safety of [ 110-30-5 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 110-30-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 110-30-5 ]

[ 110-30-5 ] Synthesis Path-Upstream   1~5

  • 1
  • [ 107-15-3 ]
  • [ 57-11-4 ]
  • [ 110-30-5 ]
YieldReaction ConditionsOperation in experiment
94.3%
Stage #1: at 100℃; for 0.166667 h; Inert atmosphere
Stage #2: for 6 h; Inert atmosphere
stearic acid 0.28percent of the composite antioxidant was added to the reaction kettle, and the mixture was slowly heated to 100 ° C after stirring for N2 and 10 min. The stearic acid was completely melted and the 0.20percent composite catalyst with the weight of ethylenediamine and stearic acid was added. Constant temperature reaction for 2 hours, And then slowly heated to 180 ° C, constant temperature reaction for 4 hours to dehydration reaction,The water generated during the reaction is taken out of N2 to stop the reaction, Cooled to 160 ° C discharge.Wherein the molar ratio of stearic acid to ethylenediamine is 1: 0.58; the antioxidant 1076 in the antioxidant,The ratio of the antioxidant DLTDP to the antioxidant T501 was 0.20: 0.36: 1; the composite catalyst was prepared by using the p-toluenesulfonic acid / SAPO-34 supported solid acid catalyst prepared in Example 1 and Example 2 and the phosphoric acid / SiO2-Al2O3 supported solid acid catalyst, the mass ratio of 1: 3.5. The yield of N,N'-ethylenebis(stearamide)
References: [1] Patent: CN105777568, 2016, A, . Location in patent: Paragraph 0024; 0025.
[2] Industrial and Engineering Chemistry, 1948, vol. 40, p. 1365.
[3] Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1976, p. 386 - 389.
[4] Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983, p. 2197 - 2200.
[5] Patent: CN105348128, 2016, A, . Location in patent: Paragraph 0015.
  • 2
  • [ 871-79-4 ]
  • [ 112-76-5 ]
  • [ 110-30-5 ]
References: [1] Langmuir, 2010, vol. 26, # 23, p. 17890 - 17895.
  • 3
  • [ 57-11-4 ]
  • [ 110-30-5 ]
References: [1] Langmuir, 2010, vol. 26, # 23, p. 17890 - 17895.
  • 4
  • [ 112-76-5 ]
  • [ 110-30-5 ]
References: [1] Langmuir, 2010, vol. 26, # 23, p. 17890 - 17895.
  • 5
  • [ 6780-13-8 ]
  • [ 57-11-4 ]
  • [ 871-79-4 ]
  • [ 110-30-5 ]
References: [1] Nippon Kagaku Zasshi, 1948, vol. 69, p. 154,156[2] Chem.Abstr., 1952, p. 3951.
 

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