[ CAS No. 1086391-06-1 ] {[proInfo.proName]}

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2D 3D

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Quality Control of [ 1086391-06-1 ]

COA NMR CNMR HPLC LC-MS

Related Doc. of [ 1086391-06-1 ]

SDS Specification

Alternatived Products of [ 1086391-06-1 ]

Product Details of [ 1086391-06-1 ]

CAS No. :	1086391-06-1	MDL No. :	MFCD11045401
Formula :	C₉H₇BrN₂O₂	Boiling Point :	-
Linear Structure Formula :	-	InChI Key :	JEPZKKWEBQAHAO-UHFFFAOYSA-N
M.W :	255.07	Pubchem ID :	45790261
Synonyms :

Safety of [ 1086391-06-1 ]

Signal Word:	Warning	Class:	N/A
Precautionary Statements:	P261-P305+P351+P338	UN#:	N/A
Hazard Statements:	H302-H315-H319-H335	Packing Group:	N/A
GHS Pictogram:

Application In Synthesis of [ 1086391-06-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Downstream synthetic route of [ 1086391-06-1 ]

[ 1086391-06-1 ] Synthesis Path-Downstream 1~12

1
[ 1086391-06-1 ]
[ 181219-01-2 ]
[ 1353254-92-8 ]

Yield	Reaction Conditions	Operation in experiment
	With sodium carbonate;dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; In 1,4-dioxane; at 100℃; for 24h;Inert atmosphere;	Step 5. Methyl 3-pyridin-4-yl-lH-indazole-5-carboxylate 4-(4;4?5,5-Tetramethyl-l53,2-dioxaborolan-2-yl)pyridine (0.965 g, 4.70 mmol), PdCl2(dppf)-CH2Cl (0.256 g, 0.314 mmol), sodium carbonate (3.14 mL, 6.27 mmol) and methyl 3-bromo-lH-indazole-5-carboxylate (0.8 g, 3.14 mmol) were taken up in 1,4-dioxane (15 mL). The flask was evacuated and back-filled with N2 (x3) before stirring at 100 C for 24 hours. Room temperature was attained, the reaction mixture was diltuted with MeOH, filtered through Celite and concentrated in vacuo.Purification of the residue by MPLC (12-100% EtOAc-hexanes) gave methyl 3- pyridin-4-yl-lH-indazole-5-carboxylate as a yellow solid.MS (APCI) calculated for Ci4Hi2N302 [M+H]+, 254; found 254 (0.92 mins).

Reference： [1]Patent: WO2011/163330,2011,A1 .Location in patent: Page/Page column 202

2
[ 1086391-06-1 ]
[ 1353254-94-0 ]

Reference： [1]Patent: WO2011/163330,2011,A1

3
[ 1086391-06-1 ]
[ 1353253-59-4 ]

Reference： [1]Patent: WO2011/163330,2011,A1

4
1H-indazole-5-carbonyl chloride [ No CAS ]
[ 1086391-06-1 ]