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Chemical Structure| 106266-06-2 Chemical Structure| 106266-06-2
Chemical Structure| 106266-06-2

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CAS No.: 106266-06-2

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Risperidone is a multiple-target antipsychotic with high affinity for 5-HT2A and D2 receptors, alpha 1, alpha 2 and H1 receptors.

Synonyms: R 64 766; Apexidone; Psychodal

4.5 *For Research Use Only !

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Product Details of Risperidone

CAS No. :106266-06-2
Formula : C23H27FN4O2
M.W : 410.48
SMILES Code : O=C1C(CCN2CCC(CC2)C3=NOC4=C3C=CC(F)=C4)=C(N=C5N1CCCC5)C
Synonyms :
R 64 766; Apexidone; Psychodal
MDL No. :MFCD00274576
InChI Key :RAPZEAPATHNIPO-UHFFFAOYSA-N
Pubchem ID :5073

Safety of Risperidone

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H301
Precautionary Statements:P301+P310
Class:6.1
UN#:2811
Packing Group:Ⅲ

Application In Synthesis of Risperidone

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 106266-06-2 ]

[ 106266-06-2 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 106266-06-2 ]
  • [ 130-85-8 ]
  • [ 160390-88-5 ]
YieldReaction ConditionsOperation in experiment
In ethanol; N,N-dimethyl-formamide; at 25 - 30℃; for 5h; 700 ml of dimethyl formamide and 16.6 gm of pamoic acid were charged in the flask. The reaction mixture was stirred for 10 minutes at 25-30°C to obtain clear solution. 35 gm Risperidone solution in 1050 ml ethanol was added to the reaction mixture at 25-30°C. The reaction mixture was stirred further for 5 hours at 25-30°C. The solid was filtered off, washed with 70 ml ethyl alcohol and dried under vacuum at 50-55°C for 12 hours.Dry weight: 42.10 gmDSC: 188°C1 H NMR in accord with structure (400 MHz, DMSO-d6+D20) 8(ppm): 8.22 (2H) s; 8.14-8.16 (2H) d; 8.00-8.03 (2H) d of d; 7.67-7.69 (4H) m; 7.29-7.33 (2H) d of t; 7.14- 7.18 (2H) t; 7.05-7.09 (2H) t; 4.77 (2H) s; 3.81 (4H) t; 3.54 (2H) m; 3.16 3.74 (12 H) m; 2.89-2.91 (4H) m; 2.75-2.78 (4H) t; 2.10-2.15 2.36-2.42 (8H) m; 2.28 (6H) s; 1.75- 1. (8H) m.Elemental analysis (wt percent) calculated for C69H70F2N8O10: C, 68.53; H, 5.83; N, 9.27. Found: C, 68.37; H, 6.00; N, 9.65.The structural characteristics were also confirmed by BRUKER' s SMART APEX Single crystal X-ray CCD Diffractometer.
  • 2
  • [ 106266-06-2 ]
  • [ 130-85-8 ]
  • risperidone hemipamoate [ No CAS ]
YieldReaction ConditionsOperation in experiment
42.1 g In ethanol; N,N-dimethyl-formamide; at 25 - 30℃; for 5.16h; Preparation of Risperidone Hemipamoate 700 ml of dimethyl formamide and 16.6 gm of pamoic acid were charged in the flask. The reaction mixture was stirred for 10 minutes at 25-30° C. to obtain clear solution. 35 gm Risperidone solution in 1050 ml ethanol was added to the reaction mixture at 25-30° C. The reaction mixture was stirred further for 5 hours at 25-30° C. The solid was filtered off, washed with 70 ml ethyl alcohol and dried under vacuum at 50-55° C. for 12 hours. Dry weight: 42.10 gm DSC: 188° C. 1 H NMR in accord with structure (400 MHz, DMSO-d6+D2O) delta(ppm): 8.22 (2H) s; 8.14-8.16 (2H) d; 8.00-8.03 (2H) d of d; 7.67-7.69 (4H) m; 7.29-7.33 (2H) d of t; 7.14-7.18 (2H) t; 7.05-7.09 (2H) t; 4.77 (2H) s; 3.81 (4H) t; 3.54 (2H) m; 3.16 & 3.74 (12 H) m; 2.89-2.91 (4H) m; 2.75-2.78 (4H) t; 2.10-2.15 & 2.36-2.42 (8H) m; 2.28 (6H) s; 1.75-1. (8H) m. Elemental analysis (wt percent) calculated for C69H70F2N8O10: C, 68.53; H, 5.83; N, 9.27. Found: C, 68.37; H, 6.00; N, 9.65.
 

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