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[ CAS No. 105191-12-6 ] {[proInfo.proName]}

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Chemical Structure| 105191-12-6
Chemical Structure| 105191-12-6
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Product Details of [ 105191-12-6 ]

CAS No. :105191-12-6 MDL No. :MFCD06738308
Formula : C9H6BrNO Boiling Point : -
Linear Structure Formula :- InChI Key :IGZHNWFLHSANSN-UHFFFAOYSA-N
M.W : 224.05 Pubchem ID :13567958
Synonyms :

Safety of [ 105191-12-6 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P305+P351+P338 UN#:N/A
Hazard Statements:H315-H319-H335 Packing Group:N/A
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Application In Synthesis of [ 105191-12-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 105191-12-6 ]

[ 105191-12-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1836-05-1 ]
  • [ 105191-12-6 ]
  • (2E)-1-(3-bromo-2-hydroxyphenyl)-3-(6-bromo-1H-indol-2-yl)prop-2-en-1-one [ No CAS ]
YieldReaction ConditionsOperation in experiment
40% With piperidine; In ethanol; at 20℃; for 5h; General procedure: To a mixture of 1H-indole-2-carbaldehyde (290 mg, 2.0 mmol, 1.0 eq.) and 1-(5-bromo-2-hydroxyphenyl)ethanone (430 mg, 2.0 mmol, 1.0 eq.) in ethanol (10 mL) was added piperidine (1 mL). The mixture was refluxed during 16 hours and then diluted with ethyl acetate after cooling to room temperature. The organic layer was washed with a 1M aqueous hydrochloric acid solution and water, dried over Na2SO4and then evaporated under reduced pressure. The residue was purified by silica gel flash-column chromatography (eluent: heptane/EtOAc, 90/10 to 80/20) to afford, after trituration with diethyl ether,7aas a red solid (160 mg, 23 percent).
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