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Chemical Structure| 1006-23-1 Chemical Structure| 1006-23-1

Structure of 1006-23-1

Chemical Structure| 1006-23-1

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CAS No.: 1006-23-1

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Product Details of [ 1006-23-1 ]

CAS No. :1006-23-1
Formula : C4H6N6O
M.W : 154.13
SMILES Code : O=NC1=C(N)N=C(N)N=C1N
MDL No. :MFCD00006096
InChI Key :XLQQJSWJHHKLOK-UHFFFAOYSA-N
Pubchem ID :70504

Safety of [ 1006-23-1 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P305+P351+P338

Application In Synthesis of [ 1006-23-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1006-23-1 ]

[ 1006-23-1 ] Synthesis Path-Downstream   1~2

  • 2
  • [ 1004-38-2 ]
  • 2,4,5,6-tetraaminopyrimidine sulfite [ No CAS ]
  • [ 1006-23-1 ]
YieldReaction ConditionsOperation in experiment
60-75% With acetic acid; sodium nitrite; In water; EXAMPLE 2 2,4,6-triamino-5-nitrosopyrimidine was prepared by dissolving 1.0 mole of <strong>[1004-38-2]2,4,6-triaminopyrimidine</strong> in 1040 ml of water and 1.5 moles of acetic acid, maintaining the temperature in the range of about 0-16 C. Then 1.0 mole of sodium nitrite was added to the reaction mixture while controlling the reaction temperature in the range of 0-20 C. To the final reaction mixture prepared above, sodium dithionite was added over a period of about 30 minutes to an hour while allowing the reaction mixture to reach 60 C. The reaction mixture was then filtered hot and the filtrate was cooled to 5 C. at which temperature the desired product crystallized from the filtrate and was separated, giving about a 60-75% yield of 2,4,5,6-tetraaminopyrimidine sulfite, which assayed about 95% pure by high pressure liquid chromatography.
 

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