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Chemical Structure| 100-76-5 Chemical Structure| 100-76-5
Chemical Structure| 100-76-5

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CAS No.: 100-76-5

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Product Citations

Product Citations

Jach, Ewelina ; Kowalska, Dorota A ; Trzebiatowska, Monika , et al.

Abstract: Organic?inorganic hybrid compounds based on quinuclidinium and metal bromides, (C7H14N)2MBr4 (M = Co, Mn, Cd), have been synthesized. Differential scanning calorimetry measurements indicate that all compounds undergo a reversible phase transition at 251 K (Co), 205 K (Mn), and 363 K (Cd) upon heating. The respective temperature dependences of the dielectric permittivity reveal anomalies, confirming the occurrence of phase transitions. Although the crystals are isostructural at room temperature, as confirmed by X-ray diffraction data, the mechanism of the phase transitions varies in each compound. The main driving force is the reorientation of quinuclidinium, resulting in the rearrangement of hydrogen bonds. Satisfactory dielectric and thermal stability properties of these materials have been demonstrated, highlighting their potential for applications in temperature sensors and switch devices.

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Product Details of [ 100-76-5 ]

CAS No. :100-76-5
Formula : C7H13N
M.W : 111.18
SMILES Code : N1(CC2)CCC2CC1
MDL No. :MFCD00006690
InChI Key :SBYHFKPVCBCYGV-UHFFFAOYSA-N
Pubchem ID :7527

Safety of [ 100-76-5 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H301-H310-H315-H318
Precautionary Statements:P501-P270-P262-P264-P280-P302+P352-P332+P313-P362-P301+P310+P330-P302+P350+P310-P305+P351+P338+P310-P405
Class:8(6.1)
UN#:2923
Packing Group:Ⅱ

Application In Synthesis [ 100-76-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 100-76-5 ]

[ 100-76-5 ] Synthesis Path-Downstream   1~5

  • 1
  • [ 100-76-5 ]
  • [ 6608-47-5 ]
  • [ 39896-06-5 ]
  • 1-Aza-bicyclo[2.2.2]octane; compound with ethenesulfonic acid [ No CAS ]
  • [ 87323-99-7 ]
  • 2
  • [ 103260-44-2 ]
  • [ 100-76-5 ]
  • 3
  • [ 5344-27-4 ]
  • [ 100-76-5 ]
  • 4
  • [ 100-76-5 ]
  • [ 126-83-0 ]
  • 1-(3-sulfo-2-hydroxypropyl)quinuclidinium inner salt [ No CAS ]
YieldReaction ConditionsOperation in experiment
77% Preparation of 1-(3-sulfo-2-hydroxypropyl) quinuclidinium, inner salt (Compound JX); A solution of 3-chloro-2-hydroxy-1-propanesulfonic acid, sodium salt (2 g, 10 mmol) in water (12 mL total volume) was added over 1 hour to a mixture of quinuclidine (1.63 g, 4.7 mmol), water (10 mL) and 1,4-dioxane (10 mL) at 80 C. The mixture was stirred at this temperature for another 2 hours after the end of the addition. The reaction mixture was concentrated then the mixture was passed over a column of Dowex 50×8 (125 g). The fractions containing the pure product were concentrated to a white solid. The solid was dried for 18 hours at 60 C. in the vacuum oven. The desired material was obtained as a white solid (1.92 g, 7.7 mmol, 77%). The 1H and 13C NMR and MS were consistent with the structure.
  • 5
  • [ 100-76-5 ]
  • [ 13195-50-1 ]
  • [ 127-08-2 ]
  • [ 1173173-98-2 ]
 

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