1-Bromooctadecane NEW
Price | $100 | $1 |
Package | 1KG | 1000KG |
Min. Order: | 1KG |
Supply Ability: | g-kg-tons, free sample is available |
Update Time: | 2023-12-26 |
Product Details
Product Name: 1-Bromooctadecane | CAS No.: 112-89-0 |
Min. Order: 1KG | Purity: 99% |
Supply Ability: g-kg-tons, free sample is available | Release date: 2023/12/26 |
Lead time: In stock | Packaging: bottle/ drum/ bucket/ IBC, as request. |
Delivery: By sea, by air, by express | Origin: Manufacturer |
1. Product information
Product Name: | 1-Bromooctadecane |
Synonyms: | 1-BROMOOCTADECANE;STEARYL BROMIDE;OCTADECYL BROMIDE;N-OCTADECYL BROMIDE;1-BROMOOCTADECANE pure;Octadecyl bromide, Stearyl bromide;1-Bromooctadecane,96%;1-Bromooctadecane ,98% |
CAS: | 112-89-0 |
MF: | C18H37Br |
MW: | 333.39 |
EINECS: | 204-013-4 |
Product Categories: | Alkyl Bromides;Monofunctional & alpha,omega-Bifunctional Alkanes;Monofunctional Alkanes |
Mol File: | 112-89-0.mol |
1-Bromooctadecane Chemical Properties |
Melting point | 25-30 °C(lit.) |
Boiling point | 214-216 °C12 mm Hg(lit.) |
density | 0.976 g/mL at 25 °C(lit.) |
refractive index | 1.462-1.464 |
Fp | >230 °F |
storage temp. | Inert atmosphere,Room Temperature |
form | Low Melting Solid |
color | Yellow |
Specific Gravity | 0.980 (20/4℃) |
Water Solubility | insoluble |
1-Bromooctadecane Usage And Synthesis |
Chemical Properties | colorless or light yellow liquid. soluble in ethanol, ether, ethyl acetate and petroleum ether, insoluble in water. Decomposes when exposed to light. It is used in organic synthesis. |
Uses | 1-Bromooctadecane is used in the preparation of shortened single-walled carbon nanotubes (s-SWCNTs). It is utilized to prepare octadecane in the presence of sodium borohydride as a catalyst. It is involved as a raw material for the preparation of dimethyldistearylammonium bromide, which is a bentonite modifier. |
Preparation | 1-Bromooctadecane is synthesized by the reaction of stearyl alcohol with hydrogen bromide. The alcohol is heated to 100°C, dry hydrogen bromide is introduced, and the reaction temperature is maintained at 100-120°C until the solution no longer absorbs hydrogen bromide. The bromide is layered, the organic phase is washed with concentrated sulfuric acid, the bromide after the acid solution is separated and mixed with an equal volume of 90% methanol, washed with ammonia to make the bromide alkaline, then washed with 90% methanol, and anhydrous Dry calcium chloride. Finally, vacuum distillation, collecting 209-211 ℃ (1.33kPa) fraction is 1-bromooctadecane, and the yield is 90%. |
Purification Methods | Twice recrystallise bromooctadecane from the melt, then distil it under vacuum three times using the middle cut. Alternatively, wash the oil with aqueous Na2SO4, then conc H2SO4 (cool) and again with aqueous Na2SO4 and then fractionally distil it. [Meyer & Ried J Am Chem Soc 55 1574 1933, Hoffmann & Smyth J Am Chem Soc 72 171 1950, IR: LeFévre et al. Aust J Chem 12 743 1959, IR: Brini-Fritz Bull Soc Chim Fr 516 1957, Beilstein 1 IV 555.] |
2. Packaging
For powders: normal is 25kgs/Drum or bag, or larger/smaller package as request.
For liquids: normal 25kgs/drum, 180-300kgs/bucket, or IBC, determined by the nature of the product.
Or smaller package 1kg/bottle, 10kgs/bottle as request.
3. Shipping
4. Contact information
For more details, pls contact us freely.
Email address : elin@fdachem.com
Mob: 86 13613820652
WhatsApp/Skype/Wechat/LINE: 86 13613820652
Company Profile Introduction
Henan Fengda Chemical Co., Ltd. is located in the High-tech Development Zone of Henan Province. Specializing in the production and sales of various fine chemical products required for industrial production, including chemical raw materials, organic raw materials, petrochemicals, chemical reagents, solvents, catalysts, and additives, etc.
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- Since: 2023-02-10
- Address: Room 01, 2288 E05, Building 14, East Henan University, Science and Technology Park, 279 Xisanhuan Ro
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