1-[1-(4-Chlorophenyl)cyclobutyl]-3-methylbutan-1-one synthesis
- Product Name:1-[1-(4-Chlorophenyl)cyclobutyl]-3-methylbutan-1-one
- CAS Number:186521-85-7
- Molecular formula:C15H19ClO
- Molecular Weight:250.76
28049-61-8
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926-62-5
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Yield:186521-85-7 81%
Reaction Conditions:
Stage #1: 1-(4-chlorophenyl)cyclobutanecarbonitrile;isobutylmagnesium bromide in toluene at 90; for 18 h;Inert atmosphere;
Stage #2: with hydrogenchloride;water at 90 - 95;
References:
Reddy, G. Om;Sarma;Chandrasekhar;Babu, J. Moses;Prasad;Raju, C.M. Haricharan [Organic Process Research and Development,1999,vol. 3,# 6,p. 488 - 492]
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5674-02-2
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140-53-4
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78-77-3
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$14.00/5g
28049-61-8
168 suppliers
$15.00/250mg
186521-85-7
16 suppliers
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