4-DIPHENYLAMINO-BENZONITRILE synthesis
- Product Name:4-DIPHENYLAMINO-BENZONITRILE
- CAS Number:20441-00-3
- Molecular formula:C19H14N2
- Molecular Weight:270.33
Yield:20441-00-3 99%
Reaction Conditions:
Stage #1: diphenylaminewith [1,1'-bis(diphenylphosphino)ferrocene]nickel(II) chloride;isopropylmagnesium chloride lithium chloride in 2-methyltetrahydrofuran;toluene at 20; for 0.166667 h;Inert atmosphere;
Stage #2: 4-Cyanochlorobenzene in 2-methyltetrahydrofuran;toluene at 100; for 8 h;Inert atmosphere;
References:
Hu, Kunjun;Gao, Yunlong;Jin, Jian [Organometallics,2022,vol. 41,# 5,p. 509 - 513] Location in patent:supporting information
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20441-00-3
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