Isobutylene oxide synthesis
- Product Name:Isobutylene oxide
- CAS Number:558-30-5
- Molecular formula:C4H8O
- Molecular Weight:72.11
115-11-7
236 suppliers
$45.00/25g
558-30-5
233 suppliers
$20.00/5G
Yield:558-30-5 90%
Reaction Conditions:
with tert.-butylhydroperoxide;molybdenum(V) chloride in 1,2-dimethoxyethane at 120; under 3750.38 Torr; for 4 h;Inert atmosphere;Reagent/catalyst;Temperature;Solvent;Pressure;
Steps:
1.1; 2.1; 3.1 Preparation of epoxy isobutane
Add 150g isobutene, 1g MoCl5, 5g ethylene glycol, 300g tert-butyl hydroperoxide (TBHP) to a pressurized reaction kettle, charge N2 to a pressure of 0.5Mpa, at 120 Reaction 4h. The yield of the product epoxy isobutane (IBO) is 90%. 172 g of epoxy isobutane with a purity of 99.5% was obtained by distillation and separation
References:
CN108047013,2020,B Location in patent:Paragraph 0033; 0035; 0038; 0040; 0043; 0045
558-42-9
205 suppliers
$8.00/5g
558-30-5
233 suppliers
$20.00/5G
123-72-8
423 suppliers
$12.32/25ML
78-84-2
375 suppliers
$10.00/25mL
115-11-7
236 suppliers
$45.00/25g
558-30-5
233 suppliers
$20.00/5G
75-91-2
192 suppliers
$26.00/100g
115-11-7
236 suppliers
$45.00/25g
558-30-5
233 suppliers
$20.00/5G
75-65-0
755 suppliers
$10.00/10ml
![1H-Cyclopropa[l]phenanthrene-1-methanol, 1a,9b-dihydro-α,α-dimethyl-](/CAS/20210305/GIF/434933-60-5.gif)
434933-60-5
0 suppliers
inquiry
558-30-5
233 suppliers
$20.00/5G
85-01-8
298 suppliers
$15.00/10g
29526-99-6
83 suppliers
$130.00/100mg
78-93-3
6 suppliers
$30.80/500ml