3,7-dihydro-3,7-dimethyl-1H-purine-2,6-dione, sodium salt synthesis
- Product Name:3,7-dihydro-3,7-dimethyl-1H-purine-2,6-dione, sodium salt
- CAS Number:1010-59-9
- Molecular formula:C7H7N4NaO2
- Molecular Weight:202.148
58-08-2
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: sodium hydroxide / water / 75 - 103 °C / Large scale
2: sodium isocyanate; acetic acid / water / 9 h / 58 - 62 °C / pH 5.5-5.6 / Large scale
3: sodium hydroxide / 1 h / 55 - 95 °C / pH 11 / Large scale
References:
CN103724348,2016,B