| Identification | Back Directory | [Name]
(-)-Sparteine sulfate pentahydrate | [CAS]
6160-12-9 | [Synonyms]
LUPINIDINE
SparteiniSulfas
Sulfate pentahydrate
SPARTEINE SULFATE PENTAHYDRATE
SPARTEINE SULFATE, CRYSTALLIZED
LUPINIDINE SULFATE PENTAHYDRATE
(-)-SPARTEINE SULFATE PENTAHYDRATE
(-)-LUPINIDINE SULFATE PENTAHYDRATE
(-)-Sparteine pentahydrate sulfate
(-)-Sparteine sulfate pentahydrate,99%
(-)-SPARTEINE SULFATE SALT PENTAHYDRATE
(-)-Sparteine sulfate pentahydrateLupinidine
(-)-Sparteine sulfate salt, Lupinidine sulfate pentahydrate
(7S,7aR,14S,14aS)-Tetradecahydro-7,14-Methanodipyrido[1,2-a:1',2'-e][1,5]diazocine sulfate pentahydrate | [EINECS(EC#)]
206-078-4 | [Molecular Formula]
C15H38N2O9S | [MDL Number]
MFCD00149333 | [MOL File]
6160-12-9.mol | [Molecular Weight]
422.54 |
| Chemical Properties | Back Directory | [Appearance]
white fine crystalline powder | [Melting point ]
133-140 °C(lit.)
| [alpha ]
-28 º (589nm, c=2, H2O 25 ºC) | [refractive index ]
-22 ° (C=5, H2O) | [storage temp. ]
2-8°C
| [solubility ]
H2O: 0.1 g/mL, clear, colorless
| [Merck ]
8737 | [CAS DataBase Reference]
6160-12-9 |
| Hazard Information | Back Directory | [Chemical Properties]
white fine crystalline powder | [Uses]
oxytocic | [storage]
Store at -20°C | [Purification Methods]
Recrystallise the sulfate from aqueous EtOH or H2O, although the solubility in the latter is high. The free (-)-base has b 173o/8mm and is steam volatile but resinifies in air. The dipicrate forms yellow needles from EtOH/Me2CO, m 205-206o [Clemo et al. J Chem Soc 429 1931; see also Bolnmann & Schuman The Alkaloids (Ed Manske) Vol 9 175 1967]. The free (±)-base has m 71-72.5o [van Tamelen & Foltz J Am Chem Soc 82 2400 1960]. [Beilstein 23 II 99, 23 III/IV 18.] |
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