Identification | Back Directory | [Name]
DIKEGULAC DIHYDRAT | [CAS]
18467-77-1 | [Synonyms]
diprogulic acid dikegulac hydrate DIKEGULAC DIHYDRAT DIKEGULAC DIHYDRATE DIACETONE-2-KETOGULONICACID Oxogulonic acid diacetonide Diacetone-2-oxo-L-gulonic acid 2,3,4,6-DIACETONE-2-KETOGULONIC ACID Diprogulic acid (and its sodium salt) DIKEGULAC MONOHYDRATE PESTANAL 250 MG 2,3:4,6-Diisopropylidene-2-keto-L-gulonic acid L-Diacetoneketogulonic acid monohydrate (DAKS) 2,3:4,6-di-o-isopropyliden-2-oxo-l-gulonic acid α-L-xylo-2-Hexulofuranosonic acid, 2,3:4,6-bis-O-(1-methylethylidene)- 2,3:4,6-bis-o-(1-methylethylidene)-alpha-l-xylo-2-hexulofuranosonicaci | [EINECS(EC#)]
242-348-8 | [Molecular Formula]
C12H18O7 | [MDL Number]
MFCD00150519 | [MOL File]
18467-77-1.mol | [Molecular Weight]
274.27 |
Hazard Information | Back Directory | [Definition]
ChEBI:Dikegulac is a member of dioxanes. | [Purification Methods]
Dissolve -DAG in Et2O, filter, dry (MgSO4) it, filter it again and evaporate to give a yellow oil. Addition of one drop of H2O induces crystallisation to the monohydrate, which also forms rhombic crystals on recrystallisation from 95% EtOH/H2O at room temperature. [Flatt et al. Synthesis 815 1979, Reichstein & Grussner Helv Chim Acta 17 311 1934, Takagi & Jeffrey Acta Crystallogr Sect B 34 2932 1978, cf Org Synth 55 80 1976, Beilstein 19/12 V 520.] |
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