| Identification | Back Directory | [Name]
4-IODOPHENYL ISOCYANATE | [CAS]
15845-62-2 | [Synonyms]
4-IODOPHENYL ISOCYANATE
4-Iodophenyl isocyanate 97%
Benzene, 1-iodo-4-isocyanato- | [Molecular Formula]
C7H4INO | [MDL Number]
MFCD00013875 | [MOL File]
15845-62-2.mol | [Molecular Weight]
245.02 |
| Chemical Properties | Back Directory | [Melting point ]
44-48 °C(lit.)
| [Boiling point ]
84°C 5mm | [density ]
1.79±0.1 g/cm3(Predicted) | [Fp ]
>230 °F
| [storage temp. ]
2-8°C | [form ]
fused solid | [color ]
White | [Sensitive ]
Moisture & Light Sensitive | [BRN ]
2716151 |
| Hazard Information | Back Directory | [Uses]
4-Iodophenyl isocyanate may be used in the preparation of:
- silicon-stereogenic silicon-bridged arylpyridinones
- N-(4-iodophenyl)cholesteryl-3-carbamate
- N-(4-iodophenyl)pregnenolone-3-carbamate
| [Preparation]
To a solution of triphosgene (3.0 g, 10 mmol) and triethylamine (2.02 g, 20 mmol) in dry benzene (30 mL), a solution of 4-iodoaniline (4.3 g, 20 mmol) in dry benzene (15 mL) was added over 20 min. During the course of the addition, the temperature of the reaction mixture was increased from ambient to reflux temperature. After refluxing for 3 h, the reaction mixture was filtered. The filtrate was concentrated to obtain a residue, which was subjected to distillation under reduced pressure to afford a colorless liquid. Yield 2.21 g (45.2%). |
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