| Identification | Back Directory | [Name]
Carbamic acid, [(7S)-5-(phenylmethyl)-5-azaspiro[2.4]hept-7-yl]-, 1,1-dimethylethyl ester | [CAS]
144282-37-1 | [Synonyms]
[(7S)-5-(Phenylmethyl)-5-azaspiro[2.4]hept-7-yl]carbamic
tert-butyl (S)-(5-benzyl-5-azaspiro[2.4]heptan-7-yl)carbamate
(S)-tert-Butyl (5-benzyl-5-azaspiro[2.4]heptan-7-yl)carbaMate
tert-butyl N-[(7S)-5-benzyl-5-azaspiro[2.4]heptan-7-yl]carbamate
[(7S)-5-(Phenylmethyl)-5-azaspiro[2.4]hept-7-yl]carbamic acid tert-butyl ester
Carbamic acid, [(7S)-5-(phenylmethyl)-5-azaspiro[2.4]hept-7-yl]-, 1,1-dimethylethyl ester
CarbaMic acid, N-[(7S)-5-(phenylMethyl)-5-azaspiro[2.4]hept-7-yl]-, 1,1-diMethylethyl ester | [EINECS(EC#)]
1806241-263-5 | [Molecular Formula]
C18H26N2O2 | [MDL Number]
MFCD17214772 | [MOL File]
144282-37-1.mol | [Molecular Weight]
302.41 |
| Chemical Properties | Back Directory | [Boiling point ]
420.5±34.0 °C(Predicted) | [density ]
1.12 | [storage temp. ]
Sealed in dry,2-8°C | [pka]
12.31±0.20(Predicted) | [InChI]
InChI=1S/C18H26N2O2/c1-17(2,3)22-16(21)19-15-12-20(13-18(15)9-10-18)11-14-7-5-4-6-8-14/h4-8,15H,9-13H2,1-3H3,(H,19,21)/t15-/m1/s1 | [InChIKey]
UCBLMUMETZZNIZ-OAHLLOKOSA-N | [SMILES]
C(OC(C)(C)C)(=O)N[C@H]1C2(CC2)CN(CC2=CC=CC=C2)C1 |
| Hazard Information | Back Directory | [Synthesis]
3.75 g of 5-benzyl-5-azaspiro[2.4]heptan-7-amine was added to the reaction flask, followed by 35 mL of ethanol, 3.75 g of triethylamine and 6.5 g of Boc2O.Stir the reaction at room temperature for 12-14 hours, concentrate, add ethyl acetate, and then use aqueous lemon solution, sodium bicarbonate solution, and saturatedWashed with brine, dried, concentrated and dried to give tert-Butyl (S)-(5-benzyl-5-azaspiro[2.4]heptan-7-yl)carbamate.The yield was 98.2%.
![Carbamic acid, [(7S)-5-(phenylmethyl)-5-azaspiro[2.4]hept-7-yl]-, 1,1-dimethylethyl ester](/NewsImg/2024-01-03/6383987749077649741893529.jpg "Carbamic acid, [(7S)-5-(phenylmethyl)-5-azaspiro[2.4]hept-7-yl]-, 1,1-dimethylethyl ester")
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